Multilayer elastomeric material filled with radiation-attenuating compounds, preparation method and uses thereof
A kind of elastomer material, elastomer technology, applied in the field of manufacture of articles for radiation protection, especially X-ray and/or gamma ray radiation
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Embodiment 1
[0054] figure 1 B is shown according to the present invention similar to figure 1 The material shown in A, but with layer L1 also having a silk screen on top of it. Example 1: Preparation of an elastomer solution for the preparation of a radiopaque intermediate layer L2
[0055] An elastomer solution B1 useful for the preparation of the radiopaque intermediate layer L2 was prepared, said solution having the following composition:
[0056] -SEBS copolymer (trade name: G1652, Kraton Polymers) 41.0g
[0057] - Paraffin oil (plasticizer) (trade name: 352, Esso) 29.0g
[0058] -Cyclohexane (total) 200.0g
[0059] - Radiopaque substance: bismuth trioxide (Bi 2 o 3 ) 318.0g
[0060] - Diluent for the emulsion of the dispersed phase: polyethylene glycol (PEG 200) 79.0 g
[0061] The continuous phase of the emulsion consists of about 13 wt% of G1652 copolymer and used as plasticizer 352 blend of mineral oils. In this mixture, the weight ratio of elastomer / plasticizer i...
Embodiment 2
[0064] Example 2: Preparation of an elastomer solution for the preparation of a radiopaque intermediate layer L2
[0065] An elastomer solution B2 useful for preparing a radiopaque intermediate layer L2 was prepared, said solution having the following composition:
[0066] - G1652 28.0g
[0067] - 352 29.0g
[0068] -Cyclohexane 224.0g
[0069] -Ortho-xylene 28.0g
[0070] -Bi 2 o 3 256.0g
[0071] - Diluent for emulsion of dispersed phase: gelatin / water / PEG 200 64.0g
[0072] The continuous phase of the emulsion consists of about 10 wt% of G1652 copolymer and used as plasticizer 352 blend of mineral oils. In this mixture, the weight ratio of elastomer / plasticizer is 100 / 100. To dissolve the copolymer / plasticizer mixture, the plasticized elastomer was contacted with the solvent for 1 hour and 30 minutes. The solvent comprised a mixture of cyclohexane (total) and o-xylene (total) in a weight ratio of 88 / 12.
[0073] The co...
Embodiment 3
[0076] Example 3: Preparation of Elastomeric Solutions for the Preparation of Radiopaque Intermediate Layers Containing Bismuth Trioxide in Two-Phase Emulsions
[0077] An elastomer solution B3 useful for the preparation of the radiopaque intermediate layer L2 was prepared, said solution having the following composition:
[0078] - G1652 40.0g
[0079] - 352 28.0g
[0080] -Cyclohexane 210.0g
[0081] -Bi 2 o 3 724.0g
[0082] - Diluent for the emulsion of the dispersed phase: PEG 200 72.0 g
[0083] Continuous phase emulsions include G1652 copolymer and used as plasticizer 352 blend of mineral oils (approximately 8% by weight relative to solids content). In this mixture, the weight ratio of elastomer / plasticizer is 100 / 70. To dissolve the copolymer / plasticizer mixture, the plasticized elastomer was contacted with the solvent for 1 hour and 30 minutes. The solvent used was cyclohexane (total). Bi 2 o 3 Added to the continuo...
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