Acrylic esters oiliness pressure-sensitive glue and preparation method thereof
A technology of acrylic esters and glues, applied in the direction of adhesive types, ester copolymer adhesives, etc., to achieve good initial adhesion and good color coverage
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[0019] The formula used in this embodiment is:
[0020] Isooctyl acrylate 35%
[0021] Butyl acrylate 10%
[0022] Vinyl acetate 15%
[0023] Acrylic 4%
[0024] Azobisisobutyronitrile 5‰
[0025] Ethyl acetate 16%
[0026] Ethanol 18%
[0027] Curing agent 5‰
[0028] Nano-level AL 5‰
[0029] Surfactant 5‰.
[0030] The preparation process steps and conditions of this embodiment are:
[0031] According to the above raw material formula, mix isooctyl acrylate, butyl acrylate, vinyl acetate, acrylic acid, azobisisobutyronitrile, ethyl acetate and ethanol uniformly, and then add them to the reactor. The addition amount is 1 / 5 of the reactor. Start heating, after reacting at 70-85°C for 1-2 hours, add the remaining reactants dropwise and complete the dropwise addition within 2-5 hours. After the dropwise addition is completed, keep it for 2-5 hours and then cool to below 50°C , Add the curing agent, and then the material can be discharged; the discharged semi-finished glue is put in...
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