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A technology of polyurethane glue and polyurethane, applied in the direction of polyurea/polyurethane adhesive, monocarboxylate copolymer adhesive, adhesive, etc., to achieve the effect of reducing storage and use temperature
Inactive Publication Date: 2009-03-25
上海九元石油化工有限公司
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Abstract
Description
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Problems solved by technology
[0002] Polyurethane adhesives with highly crystalline properties have the advantages of fast drying and good bond strength, but because of the gel problem, it seriously affects the use and storage in winter, especially in severe cold areas. In traditional applications, manufacturers and users have to build insulation Store in the room or use various heating measures before use to restore the performance of the glue
Method used
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Effect test
Embodiment 1
[0012] First add 40g of acetone, 35g of methyl ethyl ketone, 5g of cyclohexanone and 20g of ethyl acetate and mix thoroughly to form a mixed organic solvent A, then raise the temperature to 35-60°C, and gradually add 12g of grades while stirring at a speed of 600-1000 rpm The mixture B is composed of JY5020 and 10g of JY1036 polyurethane particles. React for 5-10 hours. After the particles are completely dissolved, add 1.5g of brand 4744 antifreeze modifier C, stir and mix for 1 hour, add 1g of brand for Antioxidant D of JY-Stab 8733, fully stirred for 30 minutes, cooled the system to room temperature, filtered and packaged to obtain the finished product.
Embodiment 2
[0014] First add a mixed organic solvent A consisting of 55g of acetone, 50g of methyl ethyl ketone, and 5g of toluene, mix thoroughly, then raise the temperature to 35-60°C, stir at a speed of 600-1000 rpm, and gradually add the brands of NY7503 and JY5400 , the mixture B composed of JY2120 polyurethane particles, the weights of the polyurethane particles of the above three grades are 12g, 6g, 5g respectively, react for 5-10h, and add 1g of antifreeze modifier C with the grade T1804 after the particles are completely dissolved , fully stirred and mixed for 1 hour, added 1.2 g of UV-328 ultraviolet absorber D, fully stirred for 40 minutes, lowered the system to room temperature, filtered and packaged to obtain the finished product.
Embodiment 3
[0016] First add 50g of acetone and 50g of methyl ethyl ketone mixed organic solvent A, mix well, then raise the temperature to 35-60°C, stir at 600-1000 rpm, and gradually add 22g of NY5813 polyurethane particles B , react for 5-10 hours, after the particles are completely dissolved, add 1.2g of antifreeze modifier C with the brand name T1808, stir and mix thoroughly for 1 hour, lower the system to room temperature, filter and pack to obtain the finished product.
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract
The invention relates to the macromolecule material and chemical technical field, in particular to a preparation method of an improved polyurethane glue. The preparation method is characterized in that: an organic solvent A is heated to 35DEG C to 60DEG C, stirred at 600revolution/min to 1000revolution/min and added with polyurethane grains B gradually simultaneously; the addition of the added polyurethane grains B is 20 percent to 60 percent of the weight of the organic solvent, and then reaction is carried out for 5h to 10h; after the dissolution of the grains, an anti-freezing modifier C is added, stirred and mixed; according to needs, other auxiliary agents D are added, stirred and mixed fully, and the temperature is lowered to 20 DEG C to 35 DEG C; and the macromolecule material is obtained by filtering and packaging. The addition of the anti-freezing modifier accounts for 0.01 percent to 10 percent of a finished improved polyurethane glue system according to weight percentage. The beneficial results of the preparation method includes: the improved polyurethane glue can be utilized at 15 DEG C below zero to 5 DEG C, the temperature required in storage and utilization of a crystalline polyurethane glue is reduced, thereby being widely applicable to the industries of clothes, automobiles and furnitures, and bringing fortune to a broad range of users of a similar glue in freezing regions.
Description
[technical field] [0001] The invention relates to the technical fields of polymer materials and chemical industry, in particular to a preparation method of modified polyurethane glue. [Background technique] [0002] Polyurethane adhesives with highly crystalline properties have the advantages of fast drying and good bond strength, but because of the gel problem, it seriously affects the use and storage in winter, especially in severe cold areas. In traditional applications, manufacturers and users have to build insulation Store in the room or use various heating measures before use to restore the performance of the glue. [Content of the invention] [0003] The purpose of the present invention is to enable the polyurethane glue with a highly crystalline structure to be stored and used at -15°C. [0004] In order to achieve the above purpose, a preparation method of modified polyurethane glue is designed, the composition of which is: organic solvent A, the temperature is ra...
Claims
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information
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