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Stabilizing agent of liquid single-cyandiamide and method for producing stable liquid single-cyandiamide

A cyanamide and stabilizer technology, applied in the field of stabilizers and the preparation of stable liquid cyanamide, can solve the problems such as the inability to achieve liquid cyanamide storage and transportation, and achieve the effect of solving storage and transportation problems

Inactive Publication Date: 2009-05-13
宁夏大荣化工冶金有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In order to prevent the dimerization reaction during storage and transportation, acid stabilizers must be added. At present, the stabilizers generally added are mainly phosphoric acid, formic acid, sodium dihydrogen phosphate, etc., and these stabilizers can achieve a certain stabilizing effect, but still It cannot achieve the purpose of storing and transporting liquid cyanamide at natural ambient temperature, and must be stored and transported below 10°C

Method used

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  • Stabilizing agent of liquid single-cyandiamide and method for producing stable liquid single-cyandiamide

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0011] Get 300g of cyanamide (purity 52.0%) and join in the 500mL three-neck flask that stirrer, cooling device and thermometer are equipped with, under the situation of stirring and cooling, slowly add acetic acid 4.57g. Stable liquid cyanamide can be obtained by controlling the temperature at natural ambient temperature.

Embodiment 2

[0013] Get 300g of cyanamide (purity 30.0%) and join in the 500mL three-neck flask that stirrer, cooling device and thermometer are equipped with, under the situation of stirring and cooling, slowly add acetic acid 3.03g. Control the temperature at natural ambient temperature. A stable liquid cyanamide is obtained.

Embodiment 3

[0015] Get 300g of cyanamide (purity 25.0%) and join in the 500mL three-necked flask that stirrer, cooling device and thermometer are equipped with, under the situation of stirring and cooling, slowly add acetic acid 3.03g. Control the temperature at natural ambient temperature. A stable liquid cyanamide is obtained.

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Abstract

The invention belongs to the field of chemical engineering, and particularly relates to a stabilizer for liquid cyanamide and a method for preparing stable liquid cyanamide. The stabilizer for liquid cyanamide can be acetic acid or metacetonic acid. The method for preparing stable liquid cyanamide comprises steps as follows: liquid cyanamide is put into a container with a stirring device; the stabilizer with the liquid cyanamide weight 0.01-5.0% is added slowly in stirring; the temperature of the liquid cyanamide in the container is controlled to be the natural environmental temperature; and the liquid cyanamide with stable performance is obtained. A large amount of experiments show that proper acetic acid or metacetonic acid is added into liquid cyanamide to be the stabilizer, so that liquid cyanamide can be in a very stable state at the natural environmental temperature, all of the physicochemical properties of liquid cyanamide are kept, and the long-term problems of storage and transportation of liquid cyanamide at the natural environmental temperature are solved.

Description

technical field [0001] The invention belongs to the field of chemical industry, in particular to a stabilizer for liquid cyanamide and a method for preparing stable liquid cyanamide. Background technique [0002] Cyanamide, also known as cyanamide and cyanamide, is a weak acid, but it is a very flexible compound, and it is a colorless, deliquescent, orthorhombic crystal. It has a large solubility in polar organic solvents, a small amount in non-polar solvents, and a large solubility in water. There is a cyano group and an amino group in the cyanamide molecule, which can react with a series of compounds. These reactions can be mainly divided into two categories: one is the addition reaction with the cyano group, and the other is the substitution reaction with the amino group. In aqueous solutions, these reactions depend on the pH and temperature of the medium. [0003] Polymerization reaction is one of the important reactions of cyanamide. During the storage process, cyan...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01C3/16
Inventor 赵黎明
Owner 宁夏大荣化工冶金有限公司
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