Primer composition and articles incorporating the primer
A technology for products and primers, applied in the field of primer compositions and products containing the primers, can solve problems such as coating adhesion
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[0026] This example illustrates the method of preparing the primer composition of the present invention.
[0027] A 25% solution was prepared by dissolving 91.5 g of Epon 1001F epoxy (available from Hexion Specialty Chemicals, Inc. of Houston, Texas) in 274.5 g of Dowanol PM solvent (available from Dow Chemical Company of Midland, Michigan). Add 58 g of A-1170 aminosilane (available from GE Advanced Materials in South Charleston, West Virginia), stir and react with Epon 1001F epoxy at 180°F (82°C) for 2 hours to decompose all or substantially all of the amine groups react with epoxy groups. The solution was allowed to cool to room temperature. Add 9.3g water to 738g Dowanol PM and stir. The 25% epoxy / silane solution was then added to the Dowanol PM / water solution and stirred for 1 hour. Add 337.5 g of butyl cellosolve solvent (2-butoxyethanol; commercially available from the Dow Chemical Company of Midland, Michigan) and stir to make a 10% solids primer solution. 0.4 g of ...
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