Electrolyte for the galvanic deposition of aluminium from aprotic solvents in a plating barrel
An electrolyte and aprotic technology, which is applied in the fields of compounds containing group 3/13 elements of the periodic table, chemical instruments and methods, organic chemistry, etc., can solve problems such as deficiencies, and achieve high plating ability and uniform corrosion resistance.
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[0053] Example
[0054] 1. Preparation of electrolyte
[0055] Tetraethylammonium chloride, which can be purchased as a monohydrate, is dried under vacuum. One mole of dried tetraethylammonium chloride was mixed with toluene to obtain a suspension. During cooling, 2 moles (used as pure substance or as a toluene solution) of triethylaluminum are added dropwise to the suspension. The reaction mixture was stirred. Get N(C 2 H 5 ) 4 Cl·2Al(C 2 H 5 ) 3 ·2 A clear solution of toluene. With respect to the usage amount of tetraethylammonium chloride, 2 moles of toluene was used as a solvent. The resulting product is used as an electrolyte.
[0056] 2. The conductivity of the electrolyte of the present invention is compared to the conductivity of the electrolyte of the prior art
[0057] Adequate conductivity of the electrolyte is a basic requirement for adequate coating, especially for small parts in the coating drum. The conductivity of the electrolyte of the present invention is signifi...
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