Five-stage manufacturing method of low voltage electrode foil for aluminum electrolytic capacitor
A technology for aluminum electrolytic capacitors and manufacturing methods, which is applied in the direction of electrolytic capacitors, capacitors, circuits, etc., can solve the problems of poor storage performance of electrode foils and increase the life time of capacitors, and achieve the effects of high formation efficiency, small leakage, and long life at high temperature
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[0007] Example 1:
[0008] Take the corroded low-voltage aluminum foil with a purity of 99.99%, and use a current density of 100mA / cm in a 4% ammonium adipate solution at 70°C. 2 15V into 10 minutes, and then in 4% ammonium adipate 70 ℃ aqueous solution at 100mA / cm 2 Current density, 26V into 10 minutes, and then three-stage formation, the three-stage formation conditions are the same stage formation, the formation voltage is 38V, the time is 10 minutes, and then the fourth and fifth-level formation, the chemical conversion solution is 3% hexamethylene Ammonium acid, temperature is 70℃, current density is 100mA / cm 2 , The voltage is 46V and 50V, respectively, the time is 10 minutes and 26 minutes, and then heat treatment at a high temperature of 300 ℃ for 2 minutes, followed by 3% NH 4 H 2 PO 4 Aqueous solution 70℃100mA / cm 2 After forming at 50V for 12 minutes (post forming 1), then treating in a 2% phosphoric acid solution at a temperature of 50°C, and finally performing post for...
Example Embodiment
[0009] Example 2:
[0010] Take the corroded low-voltage aluminum foil with a purity of 99.99%, and use a current density of 100mA / cm in a 10% ammonium adipate solution at 70°C. 2 15V into 10 minutes, and then 100mA / cm in 5% ammonium adipate 70℃ aqueous solution 2 Current density, 26V into 10 minutes, and then three-stage formation, the three-stage formation conditions are the same stage formation, the formation voltage is 38V, the time is 10 minutes, and then the fourth and fifth-level formation, the chemical conversion solution is 3% hexamethylene Ammonium acid, temperature is 70℃, current density is 100mA / cm 2 , The voltage is 46V and 50V, respectively, the time is 10 minutes and 26 minutes, and then heat treatment at a high temperature of 300 ℃ for 2 minutes, followed by 3% NH 4 H 2 PO 4 Aqueous solution 70℃100mA / cm 2 After forming at 50V for 12 minutes (post-forming 1), then treating in a 4% phosphoric acid solution at a temperature of 50°C, and finally performing post-formin...
Example Embodiment
[0011] Example 3:
[0012] Take the corroded low-pressure aluminum foil with a purity of 99.99%, and use a current density of 100mA / cm in an 8% ammonium adipate solution at 70°C. 2 15V into 10 minutes, and then in 4% ammonium adipate 70 ℃ aqueous solution at 100mA / cm 2 Current density, 26V into 10 minutes, and then three-stage formation, the three-stage formation conditions are the same stage formation, the formation voltage is 38V, the time is 10 minutes, and then the fourth and fifth-level formation, the chemical conversion solution is 3% hexamethylene Ammonium acid, temperature is 70℃, current density is 100mA / cm 2 , The voltage is 46V and 50V, respectively, the time is 10 minutes and 26 minutes, and then heat treatment at a high temperature of 300 ℃ for 2 minutes, followed by 3% NH 4 H 2 PO 4 Aqueous solution 70℃100mA / cm 2 After forming at 50V for 12 minutes (post-forming 1), then treating in a 4% phosphoric acid solution at a temperature of 50°C, and finally performing post-f...
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