Method for producing SiC single crystal
一种制造方法、单晶的技术,应用在单晶生长、单晶生长、化学仪器和方法等方向,能够解决未实现高的晶体生长速度、未充分满足、高生长面平滑度等问题
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[0014] Examples of the present invention are described below. In this example, a SiC single crystal was fabricated using a Si-Ti-M-C quaternary solution ("M" is Sn or Ge) by adding Ti and Sn or Ge to a Si-C2 binary solution As a result, both high growth surface smoothness and high growth speed are achieved. The addition amounts of Ti, Sn and Ge are as follows. Note that in this specification, the amount of each additive in the Si melt is expressed relative to the amount of the entire Si melt.
[0015] Ti increases the amount of C dissolved into the Si melt from the graphite crucible, thereby accelerating the growth of a single crystal. In order to obtain this effect, the addition amount of Ti needs to be at least 5 atomic % with respect to the amount of the whole Si melt. However, adding too much Ti to the Si melt may cause the resulting single crystal to have an uneven growth face. Therefore, the amount of Ti added is set to 30 atomic % or less. That is, if more than 30 ...
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