Extraction method for ginseng, ophiopogon root and schisandra chinensis and preparation thereof
The technology of Schisandra chinensis and ginseng is applied in the field of preparations for invigorating Qi and Fumai for the treatment of cardiovascular diseases and the preparation thereof, and achieves the effects of quick effect, high curative effect and good stability of finished products
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Embodiment 1
[0075] (1) Single extraction of ginseng, the extraction steps are as follows:
[0076] (1) Ginseng fibrous root coarse powder, ginseng slices, crushed into granules;
[0077] (2) Add 8 times the amount of water-containing lower alcohol, the concentration of water-containing lower alcohol is 60%, reflux extraction 6 times, each time for 3 hours, the lower alcohol is ethanol;
[0078] (3) degreasing with dichloromethane, extracting with n-butanol, concentrating the extract, combining the extract, concentrating the extract to obtain a medicinal extract, and obtaining a single extract of ginseng;
[0079] (2) Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0080] (1) Ophiopogon japonicus, crushed into granules;
[0081] (2) 90% ethanol percolation, the amount of ethanol is 18 times, the time is 24 hours, degreasing;
[0082] (3) Ophiopogon japonicus is dried to remove alcohol after percolation;
[0083] (4) Add 8 times the amount of wat...
Embodiment 2
[0097] (1) Single extraction of ginseng, the extraction steps are as follows:
[0098] (1) Ginseng fibrous root coarse powder, ginseng slices, crushed into granules;
[0099] (2) Add 8 times the amount of water-containing lower alcohol, the concentration of water-containing lower alcohol is 60%; reflux extraction 6 times, each time for 3 hours, the lower alcohol is ethanol;
[0100] (3) degreasing with dichloromethane, extracting with n-butanol, concentrating the extract, combining the extract, concentrating the extract to obtain a medicinal extract, and obtaining a single extract of ginseng;
[0101] (2) Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0102] (1) Ophiopogon japonicus, crushed into granules;
[0103] (2) 90% ethanol percolation, the amount of ethanol is 18 times, the time is 24 hours, degreasing;
[0104] (3) Ophiopogon japonicus is dried to remove alcohol after percolation;
[0105] (4) Add 8 times the amount of wat...
Embodiment 3
[0119] (1) Single extraction of ginseng, the extraction steps are as follows:
[0120] (1) Ginseng fibrous root coarse powder, ginseng slices, crushed into granules;
[0121] (2) Add 6 times the amount of water-containing lower alcohol, the concentration of water-containing lower alcohol is 45%, reflux extraction 2 times, each time for 0.5 hours, the lower alcohol is methanol;
[0122] (3) Combine the extracts, concentrate the extracts to obtain extracts, and obtain the product as a single extract of ginseng;
[0123] (2) Ophiopogon japonicus is extracted separately, and the extraction steps are as follows:
[0124] (1) Ophiopogon japonicus, crushed into granules;
[0125] (2) 85% ethanol percolation, the amount of ethanol is 12, the time is 12 hours, degreasing;
[0126] (3) Ophiopogon japonicus is dried to remove alcohol after percolation;
[0127] (4) Add 6 times the amount of water, extract 2 times at 85°C, 0.5 hours each time;
[0128] (5) Filtrate while hot, add 0.2...
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