Omega-crystal form, preparation method and medicine composite of ivabradine hydrochloride
A technology of hydrochloride and crystal form, applied in the field of ω-crystal form of ivabradine hydrochloride, its preparation and pharmaceutical composition, capable of solving problems not specifically described in detail
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Embodiment 1
[0019] Embodiment 1: the omega-crystal form of ivabradine hydrochloride
[0020] 20 grams of ivabradine hydrochloride obtained according to the method described in European patent specification EP0534859 was added to 30 ml of purified water, heated while stirring until completely dissolved. It is then cooled and freeze-dried. According to XRD it was shown that the ω-crystal form was generated.
Embodiment 2
[0021] Embodiment 2: pharmaceutical composition
[0022] Recipe for the preparation of 1000 tablets each containing 7.5 mg of febuxostat:
[0023] Compound 8.085g of Example 1
[0024] Cornstarch 30g
[0025] Mannitol 85g
[0026] PVP 11.5g
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