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Natural phospholipid compound greasing agent and preparation method thereof

A technology of natural phospholipids and fatliquor, which is applied in the directions of small hide/big hide/leather/fur treatment, leather impregnation, small hide/big hide/leather skin/fur chemical treatment, etc. It can solve the problem of easy adhesion on leather surface, Not suitable for shallow leather white leather fatliquor, pollution and other issues

Active Publication Date: 2010-09-29
QI HE LI HOU CHEM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the natural phospholipid has a darker color, so it is not suitable to be used as a fatliquoring agent for light leather white leather, and its HLB value is low, and its hydrophilicity is poor. Direct use cannot meet the fatliquoring requirements, and it is easy to adhere to the leather surface and cause pollution.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] 300kg natural phospholipid was added in the 1000L enamel reaction kettle equipped with stirrer, thermometer and condenser, be warming up to 65 ℃, add 2.5kg composite decolorizing agent, react 3 hours, obtain the natural phospholipid after decolorization; 70kg of composite emulsifier, 83kg of sulfite hoof oil, and 103kg of fatty alcohol phosphate ester, keep stirring for 1 hour, start to add 30% sodium hydroxide solution dropwise, adjust the pH value of the system to 7.5, add preheated to 80 ℃ 534kg of distilled water, stirred for 3.5 hours, cooled and discharged to obtain 1090kg of natural phospholipid compound fatliquoring agent with an oil content of 51%.

Embodiment 2

[0023] 300kg natural phospholipid was added in the 1000L enamel reaction kettle equipped with agitator, thermometer and condenser, be warming up to 65 ℃, add 2.7kg composite decolorizing agent, react 2.5 hours, obtain the natural phospholipid after decolorization; 74kg of composite emulsifier, 96kg of sulfite hoof oil, and 93kg of fatty alcohol phosphate ester, keep stirring for 1 hour, start to drip 30% sodium hydroxide solution, adjust the pH value of the system to 7.0, add preheated to 80 ℃ 597.8kg of distilled water, stirred for 3 hours, cooled and discharged to obtain 1060.8kg of natural phospholipid compound fatliquoring agent with an oil content of 48.5%.

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PUM

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Abstract

The invention provides a natural phospholipid compound greasing agent and a preparation method thereof. The natural phospholipid compound greasing agent consists of natural phospholipid, sulfitation neat's foot oil and fatty alcohol phosphate. The natural phospholipid compound greasing agent for greasing can improve the waterproof performance and fullness of leather and achieve satisfying greasing effect; and the natural phospholipid compound greasing agent is suitable for greasing light color leather due to light color. The method for preparing the natural phospholipid compound greasing agent comprises the following steps of: (1) heating natural phospholipid to between 50 and 70 DEG C, adding a compound decolorizing agent into the natural phospholipid, fully reacting the mixture for 3 to 4 hours, and then adding the following components in percentage by weight into the mixture: 7 to 10 percent of compound emulsifying agent, 7.5 to 10 percent of sulfitation neat's foot oil and 7.5 to 10 percent of fatty alcohol phosphate; keeping the temperature between 50 and 70 DEG C, stirring the components for 1 hour and mixing the components uniformly; (2) adding 30 percent sodium hydroxide solution into the grease mixture to perform neutralization, and adjusting the pH value to between 6.0 and 8.0; and (3) slowly adding a certain amount of distilled water (preheated to 80 DEG C) into the mixture to keep the oil content between 48 and 52 percent, and fully stirring the mixture for 2 to 5 hours to obtain the modified phospholipid compound greasing agent.

Description

technical field [0001] The present invention relates to a composite fatliquor and a preparation method thereof, more particularly, the present invention relates to a natural phospholipid composite fatliquor composition and a preparation method thereof. Background technique [0002] Fatliquor is the largest chemical material in leather production, and one of the important chemical materials in leather processing. It can not only lubricate the leather fibers, prevent the leather from being stiff and cracked, but also make the leather have corresponding toughness and softness, maintain its strength, and at the same time play a certain filling role to make the leather plump and elastic. One of the important factors affecting the quality and performance of leather. In the study of fatliquor, fatty alcohol phosphate ester, fatty acid higher alcohol ester, beef hoof oil, lanolin, natural phospholipid, synthetic macromolecular polyphosphate, etc. have good filling properties. Amon...

Claims

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Application Information

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IPC IPC(8): C14C9/02
Inventor 冯练享白清泉
Owner QI HE LI HOU CHEM CO LTD
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