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A kind of fish oil fatliquoring agent and preparation method thereof

A fish oil fatliquoring and oil content technology, which is applied in small raw hide/big raw hide/leather/fur treatment, leather impregnation, small raw hide/big raw hide/leather skin/fur chemical treatment, etc. It can solve the problem of easy oxidative discoloration, fish Problems such as fishy smell, limiting the scope of application of fish oil fatliquor

Active Publication Date: 2016-04-06
QI HE LI HOU CHEM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the increasing requirements for the light resistance of leather, natural fish oil contains more unsaturated bonds, is easy to oxidize and discolor, and has a fishy smell, so the application range of fish oil fatliquor is limited.

Method used

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  • A kind of fish oil fatliquoring agent and preparation method thereof
  • A kind of fish oil fatliquoring agent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] Add 23kg of high-carbon alcohol into a 50L pre-reaction kettle, heat up to 50°C, add 8.5kg of maleic anhydride under stirring, heat up to 88-92°C, react for 2 hours, and set aside; add 223.5kg of fish oil to the Add 1.5kg of antioxidant, 74kg of mineral oil, and 56.5kg of 30% aqueous solution of sulfonating agent to the 500L enamel reaction kettle with agitator, thermometer and condenser; For the materials in the kettle, continue to heat up to 85-95°C, stir for 1 hour to mix evenly; then cool down to 60-65°C, add 40kg of compound emulsifier, 0.5kg of preservative; keep the temperature at 60-65°C, add neutralizer 25.7 kg, adjust the pH value to 7-9; slowly add 10 kg of distilled water and fully stir for 2 hours, cool down and discharge to obtain 463.2 kg of fish oil fatliquor with an oil content of 70%.

Embodiment 2

[0017] Add 23kg of high-carbon alcohol into a 50L pre-reaction kettle, heat up to 55°C, add 8.5kg of maleic anhydride under stirring, heat up to 88-92°C, react for 3 hours, and set aside; add 241.3kg of fish oil into the Add 1.6kg of antioxidant, 79.8kg of mineral oil, and 61kg of 30% aqueous solution of sulfonating agent to the 500L enamel reaction kettle with agitator, thermometer and condenser; For the materials in the kettle, continue to heat up to 85-95°C, stir for 1.5 hours to mix evenly; then cool down to 60-65°C, add 43kg of compound emulsifier, 0.5kg of preservative; keep the temperature at 60-65°C, and add 27.7kg of neutralizer kg, adjust the pH value to 7-9; slowly add 19.4 kg of distilled water and fully stir for 2.5 hours, cool down and discharge to obtain 505.8 kg of fish oil fatliquor with an oil content of 72%.

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PUM

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Abstract

The invention provides a fish oil fatliquoring agent and a preparation method thereof. The fish oil fatliquoring agent of the present invention is composed of higher carbon alcohol, maleic anhydride, fish oil, antioxidant, mineral oil, sulfonating agent, compound emulsifier and preservative. The fish oil fatliquoring agent of the invention can not only improve the light resistance and fullness of leather and obtain a satisfactory fatliquoring effect, but also greatly extend the application range of the fatliquor because the fish oil fatliquoring agent has a light fishy taste. The preparation method of the fish oil fatliquoring agent is relatively simple, the requirements for equipment are not high, and the production cycle is short.

Description

technical field [0001] The present invention relates to a kind of fatliquoring agent and its preparation method, more specifically, the present invention relates to a kind of fish oil fatliquoring agent and its preparation method. Background technique [0002] Fatliquor is the most used chemical material in leather production, and it is also one of the important chemical materials in leather processing. It can not only lubricate the leather fiber, prevent the leather from becoming stiff and cracking, but also make the leather have corresponding toughness and softness, and maintain its strength. At the same time, it plays a certain filling role, making the leather plump and elastic. One of the important factors affecting the quality and performance of leather. In the study of fatliquor, fatty alcohol phosphate, fatty acid higher alcohol ester, hoof oil, lanolin, natural phospholipid, fish oil, synthetic macromolecular polyphosphate, etc. all have good filling properties. Ma...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C14C9/02
Inventor 冯练享白清泉
Owner QI HE LI HOU CHEM CO LTD
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