193 results about "High alcohol" patented technology

The present invention discloses a pretreatment method and application of an alumina-supported copper oxide-rare earth metal oxide catalyst. The pretreatment method is as follows: adding the alumina-supported copper oxide-rare earth metal oxide catalyst used for the reaction of ethanol to higher alcohols into a mixture of one or several C1-C8 alcohols, impregnating at 10-90 °C for 1-24 h, filtering to remove the excess alcohol after impregnation is completed, and then drying in an oven at 40-200 °C for 1-24 h to complete the pretreatment of the catalyst. The present invention provides the application of the alumina-supported copper oxide-rare earth metal oxide catalyst pretreated by the pretreatment method in the reaction of ethanol to higher alcohols. The pretreatment method of the present invention significantly increases the selectivity of the product higher alcohols and keeps the conversion rate of ethanol unchanged or slightly improved, thus solving the problem that it is difficult to balance both the conversion rate and selectivity in the prior art.

The invention discloses a super-hydrophobic catalyst for catalyzing aqueous phase coupling of ethanol as well as a preparation method and application of the super-hydrophobic catalyst, and aims to provide a super-hydrophobic catalyst which can effectively improve the hydrophobic performance of a pure nickel-based catalyst, promote further coupling of low-carbon alcohol to higher alcohol and improve the water phase coupling of ethanol. According to the technical scheme, the preparation method comprises the following steps: adding a nickel-based catalyst and a super-hydrophobic polymer polydivinylbenzene into a ball milling tank according to a mass ratio of 1: (0-4); and carrying out ball milling for 2-10 hours at the rotating speed of 200-600 rpm to obtain the super-hydrophobic catalyst. The catalyst is used for synthesizing high-carbon alcohol from ethanol in a water phase; belongs to the technical field of synthesis.

To provide a powder-containing cosmetic with superior stability, dischargeability and usability.SOLUTION: A cosmetic has a container having a spout with a diameter of 1 to 9 mm, filled with an oil-in-water emulsion composition. The oil-in-water emulsion composition includes (A) a specific powder, (B) a higher alcohol, (C) a surfactant, (D) oil, and (E) water.SELECTED DRAWING: None

The invention discloses a carbon-coated nickel-based super-hydrophobic catalyst as well as a preparation method and application thereof, and belongs to the technical field of catalysts and high alcohol synthesis. The preparation method comprises the following steps: dissolving nickel salt and citric acid in water, and then heating and stirring the obtained mixed solution to obtain a precursor; roasting the precursor in an inert atmosphere to obtain a carbon-coated nickel-based catalyst; and carrying out ball-milling mixing on the carbon-coated nickel-based catalyst and polytetrafluoroethylene to obtain the carbon-coated nickel-based super-hydrophobic catalyst. According to the invention, the carbon-coated nickel-based catalyst is firstly prepared, then the carbon-coated nickel-based catalyst is coupled with the hydrophobic polymer polytetrafluoroethylene to form a new super-hydrophobic catalyst, and the nickel-based catalyst and the polytetrafluoroethylene are subjected to ball-milling mixing, so that the hydrophobic property of the nickel-based catalyst is improved, the water poisoning phenomenon of the catalyst is relieved, and further coupling of low-carbon alcohol to higher alcohol is promoted; the yield of the high alcohol and the selectivity of the C6 < + > high alcohol are improved, and the method has a wide application prospect.

The utility model discloses a biosafety cabinet capable of double-layer filtration, which comprises a cabinet body, an operation chamber is arranged in the cabinet body, and a bottom air duct is arranged at the bottom end of the operation chamber. By arranging the reducing pipe, the exhaust pipe, the exhaust outlet, the filter box, the exhaust filter, the air disc and the high alcohol, double-layer filtration of exhausted air is achieved, air can be exhausted into the reducing pipe through operation of the exhaust fan, airflow can be concentrated and pressurized through arrangement of the reducing pipe, meanwhile, the air is conveyed into the filter box, and the filtering effect is improved. The air disc divides air into a plurality of small bubbles and increases the contact area with the high-alcohol, the high-alcohol can kill bacteria in the air and adsorb particle dust and various suspended solids, then the air is conveyed into the air exhaust opening, secondary filtering is conducted when the air passes through the air exhaust filter, and the exhausted air is purified; therefore, the exhausted air does not carry germs, the environment is prevented from being polluted, and the use safety is improved.

The invention relates to saccharomyces cerevisiae and application thereof in wine brewing. The saccharomyces cerevisiae strain is saccharomyces cerevisiae Y24 and is preserved in the general microbiological center of the China Committee for Culture Collection of Microorganisms on March 10, 2025, and the preservation number of the saccharomyces cerevisiae strain is CGMCC (China General Microbiological Culture Collection Center) NO. 33773. The saccharomyces cerevisiae strain is a saccharomyces cerevisiae strain. The saccharomyces cerevisiae Y24 strain can grow under the conditions that the alcoholic strength is 18% vol, the pH value is 2, the sugar content is 60% and the temperature is 4 DEG C, has good high-alcoholic strength, high-acid and high-sugar endurance capacity, and meets the low-temperature fermentation requirement of wine. Meanwhile, in wine fermented by the saccharomyces cerevisiae Y24 strain, the content of dry extracts capable of enriching wine bodies is higher, the content of aroma components is higher, and the content of undesirable component methanol is lower.

The invention discloses a tandem catalysis method for improving the catalytic efficiency of preparing higher alcohol by CO2 hydrogenation, which comprises the following steps: two sections of fixed bed reactors are connected in series, the first section of reactor is filled with a catalyst for preparing olefin by CO2 hydrogenation, and the second section of reactor is sequentially filled with an olefin hydroformylation catalyst and a catalyst for preparing alcohol by aldehyde hydrogenation. According to the invention, segmented catalysis is carried out on the complex process of preparing higher alcohols through CO2 hydrogenation, and a catalyst for preparing olefins through CO2 hydrogenation, a hydroformylation catalyst and an aldehyde hydrogenation catalyst are respectively arranged in an upstream-segment reactor and a downstream-segment reactor, so that the efficiency and selectivity of preparing higher alcohols through CO2 hydrogenation are improved; through tandem catalysis, the selectivity of by-product hydrocarbons can be effectively reduced, the utilization rate of carbon is improved, the selectivity and space-time yield of higher alcohols are remarkably improved, and the separation cost of products is reduced.

The invention relates to saccharomyces cerevisiae and application thereof in wine brewing. The strain is Saccharomyces cerevisiae Y26, and is preserved in the general microbiological center of the China Committee for Culture Collection of Microorganisms on March 10, 2025, and the preservation number is CGMCC NO.33774. The invention further discloses a preparation method of the Saccharomyces cerevisiae strain. The saccharomyces cerevisiae Y26 strain can grow under the conditions that the alcoholic strength is 18% vol, the pH value is 2, the sugar content is 60% and the temperature is 4 DEG C, has good high-alcoholic strength, high-acid and high-sugar endurance capacity, and meets the low-temperature fermentation requirement of wine. Meanwhile, in wine fermented by the saccharomyces cerevisiae Y26 strain, the content of dry extracts capable of enriching wine bodies is higher, the content of aroma components is higher, and the content of undesirable component methanol is lower.

The invention provides an anaerobic gas-feeding bacterium capable of converting synthesis gas into an alcohol compound, the anaerobic gas-feeding bacterium is a Clostridium autoethanogenum E53 strain, and the preservation number of the anaerobic gas-feeding bacterium is CGMCC (China General Microbiological Culture Collection Center) No.46261. The invention further provides a preparation method of the anaerobic gas-feeding bacterium. According to the invention, a Clostridium autoethanogenum E53 strain with high alcohol yield is obtained through chemical mutagenesis screening, through optimization of culture conditions, especially addition of sodium bicarbonate in a culture system and control of the pH value of the culture system, the highest concentration of thalli fermented by anaerobic aerophagetes E53 and the capability of fermenting and accumulating alcohols are improved, the maximum cell concentration of the E53 strain can reach OD600nm-2.1 Abs, and the highest alcohol yield is 7.5 g / L.

A cosmetic composition or a fiber treatment composition for head decoration products, the composition containing (A) a cationic polymer having a viscosity when in a 1 mass% aqueous solution form at 30°C of 1000 mPa·s or more, (B) an anionic polymer, (C) one or more modified silicones selected from the group consisting of a polyglycerol-modified silicone and an amino-modified silicone, (D) a dimethylpolysiloxane, (E) a cationic surfactant, and (F) a higher alcohol, wherein a mass ratio [(A) / (B)] of the component (A) to the component (B) is 4.5 or more.

The invention provides a synthesis method of methyl hypophosphorous acid monoalkyl ester, which aims at solving the problems of high alcohol consumption, large byproduct chlorinated alkyl compounds, high product separation difficulty, large byproduct salt after an acid-binding agent is added, high process risk and the like in the existing synthesis process of methyl hypophosphorous acid monoalkyl ester, and belongs to the technical field of organic. Wherein one molecule of water is used for replacing one molecule of alcohol, while the methyl phosphorus dichloride and the alcohol are subjected to nucleophilic substitution reaction, the methyl phosphorus dichloride and the water are subjected to nucleophilic substitution reaction, and the methyl hypophosphorous acid monoalkyl ester and the byproduct bimolecular hydrogen chloride are directly obtained. Finally, on the premise of ensuring the reaction rate and the product yield, the amount of reaction byproducts is reduced, the separation difficulty is reduced, and the risk in the product separation and device operation process is reduced, so that the overall cost of synthesizing the methyl hypophosphorous acid monoalkyl ester is greatly reduced.

The invention provides lactobacillus coryniformis Z5-1 as well as a culture method and application thereof, and belongs to the technical field of food fermentation. The preservation number of the lactobacillus clavuliformis Z5-1 is CGMCC (China General Microbiological Culture Collection Center) No.31547, the lactobacillus clavuliformis Z5-1 is preserved in the China General Microbiological Culture Collection Center (CGMCC) on August 5, 2024, and the lactobacillus clavuliformis Z5-1 has good degradation and conversion effects on ethanol. The lactobacillus clavuliformis Z5-1 is inoculated in a high-alcohol-degree or other fermentation environment, so that ethanol in the environment can be effectively degraded, or ethanol generated in the fermentation process is converted into various flavor substances, and the quality of fermented food is improved; and the strain culture mode is simple and convenient to operate, low in cost and easy to popularize and apply in laboratories and industrial production.

The invention discloses a method for efficiently extracting high-purity chlorogenic acid and chlorogenic acid substances from stevia rebaudiana. The method comprises the following steps: concentrating stevia rebaudiana extract liquid to obtain permeate liquid I and trapped liquid I; adjusting the pH of the trapped fluid I to obtain a to-be-treated fluid; treating the liquid to be treated by adopting an electrodialysis-ultrafiltration coupling device, and collecting an ion phase I, an ion phase II and a desalted phase; adsorbing the ion phase II by adopting macroporous adsorption resin, and respectively analyzing by adopting a low-alcohol solution and a high-alcohol solution to obtain a low-alcohol analysis solution and a high-alcohol analysis solution; concentrating the high-alcohol desorption solution to obtain trapped fluid II, mixing and crystallizing the trapped fluid II and chlorogenic acid seed crystals, filtering to obtain filtrate I and a filter cake I, refining the filter cake I to obtain filtrate II and a filter cake II, and drying the filter cake II to obtain high-purity chlorogenic acid; concentrating the ion phase I to obtain trapped fluid III, and performing thermal concentration and spray drying on the trapped fluid III to obtain the chlorogenic acid substances. According to the method, the stevia rebaudiana is used as a raw material, high-content chlorogenic acid and chlorogenic acid substances are obtained, less waste liquid and waste materials are generated in the whole process, and the method is more environmentally friendly.

The invention discloses a method for regulating and controlling the total acid content of primary liquor in Maotai-flavor liquor brewing, and belongs to the technical field of liquor brewing. Red tassel glutinous sorghum is crushed until the crushing degree is 10%-20%, preferably 13%-15%; the method comprises the following steps: mixing the crushed sorghum and fermented grains obtained after sand fermentation according to a mass ratio of 1: 1, and cooking in retort type gelatinization equipment at a conventional gelatinization temperature for 105-120 minutes, preferably 110 minutes; by adopting the method disclosed by the invention, the content of acetic acid in the fermented grains is obviously reduced by 13.82% at the end of fermentation, the content of acetic acid and the content of total acid in primary wine are respectively obviously reduced by 9.68% and 14.47%, the content of lactic acid is not obviously changed, the content of normal propyl alcohol is synchronously obviously reduced by 14.96%, and the content of other higher alcohols is stable. The method is simple in process, does not need new equipment, is completely compatible with the existing production line, and can effectively stabilize and improve the quality of the primary wine base.

The invention relates to a method for producing higher alcohols. The invention also relates to a reaction mixture and a method for producing at least one higher alcohol, said method comprising a reaction mixture comprising a mixed culture of a first and a second microorganism in an aqueous medium comprising carbon monoxide gas, wherein the first microorganism is an acetogenic microorganism capable of converting a carbon source to acetic acid and / or ethanol; and-the second microorganism is selected from the group consisting of Clostridium kluyveri capable of converting acetic acid and / or ethanol to form an acid, and C. carboxidivorans; wherein the first microorganism is further capable of converting the acid to the corresponding higher alcohol, and the higher alcohol comprises at least 6 carbon atoms.

According to the fermented wine rich in alcohol and sweetness and the preparation process thereof, high-sugar-degree grain liquid (wort) is adopted as a fermentation substrate, fermentation is controlled through functional strains in a labor division and staged mode, and the technical problems that in a traditional process, glycerol synthesis is limited, and a wine body is thin, sour and astringent are effectively solved. The content of glycerol is increased under the pure fermentation condition, meanwhile, the content of by-products such as residual sugar and acetic acid is reduced, and high alcoholic sweetness and wine flavor coordination are synchronously achieved in a pure biological fermentation framework.

This invention belongs to the field of alcoholic beverage processing technology, specifically relating to a high-purity ginkgo wine and its preparation method. The preparation method comprises the following steps: ginkgo slurry undergoes preliminary enzymatic hydrolysis with neutral protease and amylase, followed by secondary enzymatic hydrolysis with pectinase and sodium bisulfite; brewing yeast fermentation broth is added for pre-fermentation; glutamine transaminase, *Saccharomyces cerevisiae* fermentation broth, and *Candida valerate* fermentation broth are added for post-fermentation; and finally, distillation and filtration are performed to obtain the ginkgo wine. This invention achieves complete decomposition and fermentation of ginkgo kernels through a two-step enzymatic hydrolysis and two-step fermentation process. The preparation method has advantages such as simple process and low cost, which is beneficial for industrial production; the prepared ginkgo wine has advantages such as clarity, strong aroma, high alcohol content, and low acidity.

The present invention relates to a nitrogen-doped carbon-wrapped nickel catalyst for synthesis of higher alcohols by assembly of bioethanol and a preparation method therefor. The preparation method includes the following steps: S1, subjecting a soluble nickel salt and polyacrylamide to stirring with water, completely dissolving and then drying to obtain a precursor, where a molar ratio of the soluble nickel salt to polyacrylamide is 1:(0.5-8); and S2, subjecting the precursor to pyrolysis in an inert atmosphere at 300° C.-800° C. for 1-6 hours to obtain the nitrogen-doped carbon-wrapped nickel catalyst. The catalyst prepared by the method of the present invention has an active phase with high dispersity which enables synthesis of higher alcohols by efficient assembly of small molecules, and has relatively high stability which can still maintain high conversion rate and high yield for organic phase after 10 times of repeated use.

This film-forming composition for skin contains the following components (A) to (E). A phospholipid (A) A sterol ester (B) A C10-24 higher alcohol (C) Water (D) Water-insoluble fibers (E) having an average fiber diameter of 0.3 μm to 5 μm and an average fiber length of 20 μm to 300 μm In the film-forming composition for skin, the mass ratio (B) / (E) of component (B) to component (E) is 1 to 15. The water-insoluble fibers of component (E) preferably have a variation coefficient value of the fiber length of 40% to 100%.

To provide a beer-taste beverage with a high alcohol content and improved smoothness and drinkability.SOLUTION: A beer-taste beverage has an alcohol content of 10 v / v% or more, an ethyl caproate content of 0.7 mg / L or more, and a linalool content of 5 μg / L or more.SELECTED DRAWING: None

The invention relates to a composite catalyst and a preparation method thereof. The composite catalyst can be used for promoting long-chain alpha-olefin and a synthesis gas raw material to be subjected to continuous hydroformylation-hydrogenation reaction in one step to obtain a high-carbon alcohol product. Derived cobalt and graphite-phase carbon nitride in different proportions are compounded, the electronic effect is regulated and controlled, a high-dispersion and high-activity catalytic center is formed, and the composition of a product is effectively changed. The scheme provided by the invention has the advantages of simple preparation, controllable product, high alcohol selectivity and the like, and has a large-scale application and popularization prospect.

The present application belongs to the technical field of food safety rapid detection, and discloses a liquor harmful substance synchronous identification method based on gas phase diffusion pretreatment. The present application utilizes the physical characteristics that the volatility of methanol and formaldehyde is significantly higher than that of ethanol and esters, carries out gas phase diffusion pretreatment under the condition that a closed container is at 40 DEG C to 60 DEG C, makes methanol and formaldehyde preferentially volatilize and be captured by two independent absorption chromogenic liquids respectively, makes ethanol and esters mainly remain in the liquor sample liquid, and the ethanol concentration in the absorption liquid is relatively reduced. Thus, the chromogenic reaction is carried out in the absorption liquid system in which the ethanol concentration is significantly reduced, and it is not necessary to dilute the liquor sample to low alcohol degree in a large amount, so that the technical problem that the traditional colorimetric method is seriously interfered by high alcohol degree ethanol and ester matrix is fundamentally solved.

A method for producing a higher alcohol from a waste plastic feedstock is disclosed, comprising: (a) providing a hydrocarbon feed stream comprising a pyrolysis oil feed obtained from pyrolysis of plastic waste, wherein the pyrolysis oil comprises at least 20 wt % higher olefins with a carbon number in the range C5-C20, based on its total hydrocarbon content; (b) contacting the hydrocarbon feed stream with synthesis gas under hydroformylation conditions in the presence of a hydroformylation catalyst and recovering a hydroformylation product; (c) subjecting the hydroformylation product to hydrogenation and / or a distillation to recover a higher alcohol product.

The invention relates to compositions and methods for stabilizing and enhancing the viscosity of semisolid compositions, and to the production of stabilized alcohol-containing semisolid food products. More specifically, embodiments of the invention relate to novel stabilizers for semisolid compositions, to alcohol-containing semisolid food compositions comprising them, and to processes for the preparation and use thereof. Further, the invention in embodiments thereof provides non-liquid food products containing a high alcohol content, which are stable at room temperature and do not necessitate the use of gelling agents or other chemical stabilizers.

The present invention aims to provide a manufacturing method that allows for the production of a hair conditioner containing a cationic surfactant and a higher alcohol, forming an α-gel, without the need to adjust heating or cooling rates. [Solution] A method for producing a hair conditioner, comprising the step of mixing a composition (A) with a melting point of 50°C or higher with water at 5 to 45°C, wherein the composition (A) contains a cationic surfactant and a higher alcohol. The molar ratio of the cationic surfactant to the higher alcohol (catenic surfactant:higher alcohol) is 1:1 to 1:15.

The present invention belongs to the technical field of organic synthesis, and in particular to a Ni-Bi bimetallic catalyst and its catalytic one-step synthesis of higher alcohols from ethanol. In order to develop a catalyst capable of improving the yield of C6+ higher alcohols, the present invention provides a Ni-Bi bimetallic catalyst and a preparation method thereof, wherein NiBi is alloyed by introducing bismuth atoms, so that the arrangement of atoms on the nickel surface is reconstructed, the metal Ni electronic environment is regulated, and then the catalytic performance of the catalyst Ni active center is regulated, so that the Ni-Bi bimetallic catalyst has high load, low particle size, and high directional reaction activity for higher alcohols, and is applied in the reaction of catalytic one-step synthesis of higher alcohols from ethanol, showing excellent catalytic efficiency, high reaction activity and high selectivity for high-value C6+ higher alcohol products. In addition, the present invention is simple to prepare, low in cost, and more conducive to its production application.

The invention relates to a high-alcohol-tolerant salt-tolerant microorganism Jezhou bacillus and application thereof, and belongs to the technical field of microorganisms. The preservation number of the Jejubacter sp. DT01IM3 is CGMCC (China General Microbiological Culture Collection Center) No.28463, and the preservation number of the Jejubacter sp. The Jezhou bacillus DT01IM3 can normally grow under the conditions of relatively high salt concentration (0-150g / L) and relatively high higher alcohol concentration (0-8000mg / L), and the problem of tolerance of microorganisms to higher alcohols is solved, so that a foundation is laid for producing higher alcohols by the microorganisms.

Provided is a powder cosmetic having excellent impact resistance, usability, and adhesion. This powder cosmetic contains (a) a powder, (b) 0-15 mass% inclusive of an oil component, (c) more than 0-19 mass% inclusive of a polyol, and (d) 0.1-10 mass% inclusive of a higher alcohol, the total content of the (b) oil component, the (c) polyol, and the (d) higher alcohol being 5.0-20 mass% inclusive, and the content of the (b) oil component, the (c) polyol, and the (d) higher alcohol being 0.1-10 mass% inclusive. The ratio of the amount obtained by adding the content of the polyol (c) and the content of the higher alcohol (d) to the total content is 0.10-1.0 (inclusive).

An aerosol composition including an aerosol stock solution containing a cationic surfactant (A) and a linear saturated higher alcohol (B), and a propellant (C) containing carbon dioxide. The component (A) containing a mono-long-chain-alkyl cationic surfactant (A1). A content of the component (A) being 0.9% by mass or more and less than 6.0% by mass in the aerosol stock solution. A molar ratio [(B) / (A1)] of the component (B) with respect to the component (A1) being 3.0 or more and 7.0 or less in the aerosol stock solution. A content of the component (A1) in the component (A) being 90% by mass or more and 100% by mass or less, and a difference between a number of carbon atoms of the long-chain alkyl in the component (A1) and the number of carbon atoms of the component (B) being 0.

The invention discloses a preparation method of a catalyst for producing biological aviation kerosene by using high alcohol as a raw material and adopting a slurry reactor. The preparation method comprises the following steps: (1) respectively dissolving a nickel source and an organic amine source in methanol; slowly dripping the methanol solution of the organic amine source into the methanol solution of the nickel source under stirring; after dropwise adding, heating and carrying out reflux reaction for 30-90 minutes; filtering while hot, washing with methanol, collecting solid, and drying in vacuum to obtain the organic nickel catalyst. (2) respectively acidifying aqueous solutions of an organic amine source and a molybdenum source with diluted hydrochloric acid until the pH is 2-4; slowly dripping the acidified organic amine source into the acidified molybdenum source under stirring; after dropwise adding, stirring and reacting for 30-90 minutes; filtering, washing, collecting solids, and drying in vacuum to obtain the organic molybdenum catalyst. And (3) compounding the organic nickel catalyst and the organic molybdenum catalyst according to the mass ratio of 1: (1-10) to obtain the catalyst. The catalyst is simple in preparation process and low in energy consumption, and has high catalytic activity and high hydrodeoxygenation selectivity when being used for producing biological aviation kerosene by using high-carbon alcohol as a raw material and adopting a slurry reactor.