Article having antifouling properties and intended to be used in aquatic applications, particularly marine applications
A product and performance technology, applied in the field of structural growth, can solve problems such as toxicity and pollution
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[0193] 1) Preparation of catalysts (5) and (6) according to the present invention
[0194] a) Synthesis of catalyst (5): [Zn (isopropyl acetoacetate) 2 ] or [Zn(iPr-AA) 2 ], where iPr-AA = isopropyl acetoacetate anion or enolate anion of isopropyl acetoacetate
[0195] A 97% solution of 100 mmol sodium methoxide (6.12 g) in 100 ml isopropanol was concentrated 20% by distillation, then 95% 100 mmol isopropyl acetoacetate (15.93 g) was added and the solution was heated at 80 °C for 1 Hours, an orange homogeneous solution was produced. A solution of zinc chloride (50 mmol, 7 g) in 50 ml isopropanol was then added at 70° C. within 1 hour. Heating is maintained between 80 and 90° C. for 3 hours and 30 minutes, and then, after cooling, the sodium chloride formed is filtered. The alcoholic solution was evaporated to dryness to obtain 25.3 g of a paste which was dissolved in 200 ml of ethanol. After hot filtration and evaporation to dryness, 17.2 g of white solid were obtained ...
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