The invention belongs to the field of preparation of nano composite materials, and relates to a method for preparing a NiCo2O4/graphene supercapacitor material with a microwave method. The main steps includes: using natural graphite as a raw material, oxidizing with a Hummers method to obtain graphite oxide, ultrasonically dispersing the graphite oxide in water, then adding cobalt chloride and nickel chloride, stirring and then adding urea, continuing to stir, then heating the mixed solution in a microwave reactor to 100 DEG C and carrying out a reflux reaction for 5 to 25 min, thereby obtaining a precursor, and calcining the precursor in an air atmosphere at 300 DEG C for 2h, thereby obtaining a porous flaky NiCo2O4/graphene supercapacitor material. The prepared composite supercapacitor material is synthesized through the microwave method, the preparation method is simple in technology, convenient to operate, high in feasibility, and rapid and efficient, and is easy to realize industrial implementation. The synthesized NiCo2O4 is tightly attached to the graphene, and excellent electrochemical performance is represented.