Double high laminated concentrating flux plate and preparation method thereof
A magnetically conductive plate and high-level technology, applied in the direction of chemical instruments and methods, magnets, layered products, etc., can solve the problems of low strength, unsatisfactory, expensive, etc., and achieve the effect of high magnetic permeability
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Embodiment 1
[0025] 1. Prepare raw materials:
[0026]
[0027] 2. Preparation of adhesive
[0028] Mix the raw materials ①-⑤ according to the formula, then raise the temperature to 80°C and start stirring, and at the same time reflux, the reflux temperature increases step by step, the temperature difference of each level is 15°C, and the holding time of each level is 2-3 Hours, when it rises to 200°C, keep it warm at 200±5°C for 3-5 hours to the end of the reaction; then add the raw material ⑥ and stir to dissolve for 1 hour, then cool to 50°C, and filter;
[0029] The method for determining the end point of the reaction is as follows: take a 1g sample, and use a knife method to test that the gelation time at 250±2° C. is 2-3 minutes.
[0030] 3. Preparation of magnetic powder
[0031] Mix ⑦-⑩ evenly.
[0032] 4. Glass Butterwax
[0033] Use glass cloth to carry out dewaxing in dewaxing machine, the temperature of dewaxing is 380 ℃, and the vehicle speed is 4 m / min.
[0034] 5. Us...
Embodiment 2
[0039] 1. Prepare raw materials:
[0040]
[0041] 2. Preparation of adhesive
[0042] Mix the raw materials ①-⑤ according to the formula amount, then raise the temperature to 80°C and start stirring, and at the same time reflux it, the reflux temperature increases step by step, the temperature difference of each level is 25°C, and the holding time of each level is 3 hours. When it rises to 200°C, keep it warm at 200±5°C for 3-5 hours until the end of the reaction; then add raw material ⑥ and stir to dissolve for 1 hour, then cool to 50°C and filter;
[0043] The method for determining the end point of the reaction is as follows: take a 1g sample, and use a knife method to test the gelation time at 250±2°C for 2-3 minutes.
[0044] 3. Preparation of magnetic powder
[0045] Mix ⑦-⑩ evenly.
[0046] 4. Glass Butterwax
[0047] Use glass cloth to carry out dewaxing in dewaxing machine, the temperature of dewaxing is 430 ℃, and the vehicle speed is 4-5 m / min.
[0048] 5. ...
Embodiment 3
[0053] 1. Prepare raw materials:
[0054]
[0055] 2. Preparation of adhesive
[0056] Mix the raw materials ①-⑤ according to the formula, then raise the temperature to 80°C and start stirring, and reflux at the same time, the reflux temperature increases step by step, the temperature difference of each level is 20°C, and the holding time of each level is 2.5 hours. When it rises to 200°C, keep it warm at 200±5°C for 3-5 hours until the end of the reaction; then add raw material ⑥ and stir to dissolve for 1 hour, then cool to 50°C and filter;
[0057] The method for determining the end point of the reaction is as follows: take a 1g sample, and use a knife method to test the gelation time at 250±2°C for 2-3 minutes.
[0058] 3. Preparation of magnetic powder
[0059] Mix ⑦-⑩ evenly.
[0060] 4. Glass Butterwax
[0061] Use glass cloth to carry out dewaxing in dewaxing machine, the temperature of dewaxing is 380-430 ℃, and the vehicle speed is 4.5 m / min.
[0062] 5. Appl...
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