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Method for preparing isometric crystal high temperature alloy casting alloy/ceramic interface reaction test sample

A technology of superalloy and interface reaction, applied in the field of superalloy precision casting, can solve the problems of low test efficiency, error, inability to judge reaction time, etc., and achieve the effect of improving test efficiency, improving test efficiency and saving test materials

Active Publication Date: 2013-07-17
GUIYANG AVIC POWER PRECISION CASTING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Its disadvantages are as follows: first, errors occur due to the inability to visually observe the reaction product and the reaction interface; second, the influence of the reaction temperature can only be judged, and the reaction time cannot be judged
Its disadvantages are: first, it can only judge the influence of reaction temperature but it is difficult to consider the influence of reaction time; second, it needs to pour multiple furnace castings or test rods, and the test efficiency is low

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] The equiaxed crystal hollow casting is made of nickel-based superalloy K4648 with high Cr content. The concrete steps that adopt technical scheme of the present invention are as follows:

[0024] (1) Preparation of shell type

[0025] A shell mold for directional solidification with two ceramic cores inside is prepared by traditional investment casting technology;

[0026] (2) Heating and insulation of shell type

[0027] Heat the shell in the heater of the directional solidification vacuum induction furnace to the temperature at which the alloy / ceramic interface reaction is expected to occur, set the temperature at 800°C, and keep it warm for 10 minutes;

[0028] (3) Remelting and pouring

[0029] Remelt the high-temperature alloy ingot, and when the holding time of the shell mold reaches 10 minutes, pour the alloy liquid into the cavity of the shell mold at a temperature not lower than the alloy liquidus line, and the pouring temperature is 1500°C;

[0030] (4) Di...

Embodiment 2

[0035] The equiaxed crystal hollow casting is made of nickel-based superalloy K4648 with high Cr content. The concrete steps that adopt technical scheme of the present invention are as follows:

[0036] (1) Preparation of shell mold: a shell mold for directional solidification with 6 ceramic cores inside is prepared by traditional investment casting process;

[0037] (2) Heating and heat preservation of the shell: heat the shell in the heater of the directional solidification vacuum induction furnace to the temperature at which the alloy / ceramic interface reaction is expected to occur, set the temperature at 1500°C, and keep it warm for 30 minutes:

[0038] (3) Remelting and pouring

[0039] Remelt the high-temperature alloy ingot, and when the holding time of the shell mold reaches 30 minutes, pour the alloy liquid into the cavity of the shell mold at a temperature not lower than the alloy liquidus line, and the pouring temperature is 1500°C;

[0040] (4) Directional solidi...

Embodiment 3

[0045] The material of the equiaxed crystal hollow casting is high-Cr content cast nickel-base superalloy K4648, and the specific steps of adopting the technical solution of the present invention are as follows:

[0046] (1) Preparation of shell type

[0047] A shell mold for directional solidification with 6 ceramic cores inside is prepared by traditional investment casting technology;

[0048] (2) Heating and heat preservation of the shell: heat the shell in the heater of the directional solidification vacuum induction furnace to the temperature at which the alloy / ceramic interface reaction is expected to occur, set the temperature at 1550 ° C, and keep it warm for 30 minutes;

[0049] (3) Remelting and pouring

[0050] Remelt the high-temperature alloy ingot, and when the holding time of the shell mold reaches 30 minutes, pour the alloy liquid into the cavity of the shell mold at a temperature not lower than the alloy liquidus line, and the pouring temperature is 1550°C; ...

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Abstract

The invention relates to a method for preparing an isometric crystal high temperature alloy casting alloy / ceramic interface reaction test sample, which comprises the following steps of: preparing a shell mold in which ceramic cores are arranged by the traditional investment casting process; heating the shell mold in a heater of a directional solidification vacuum induction furnace to different temperatures at which alloy / ceramic interface reaction is expected to be performed, and preserving heat; remelting a high temperature alloy ingot, pouring into a cavity of the shell mold, and pulling the heater out at a certain speed to form directional solidification castings or test samples with the cores; and cutting the directional solidification castings or test samples at different heights to acquire data of alloy and ceramic which react at the same temperature for different time. The method has the advantages that: the interface reaction time can be steplessly changed according to sampling positions, so that test efficiency is improved; the interface reaction results of the ceramic cores with different components can be obtained in one module at the same time; and the interface reaction condition can be visually observed by a microscope, so that reaction products and a reaction mechanism are determined, and the actual production of the isometric crystal castings is instructed.

Description

technical field [0001] The invention is a method for preparing equiaxed superalloy casting alloy / ceramic interface reaction sample, [0002] It belongs to the field of high-temperature alloy precision casting. Background technique [0003] Gas turbine engines have become an important prerequisite and bottleneck for the development of my country's aircraft and even large aircraft. Superalloys and their parts forming technology have always been called the heart of gas turbines and have been used to manufacture gas turbine hot end components. Many structural castings used as gas turbines mostly use equiaxed superalloys, and some castings are complex and have a hollow structure, and sometimes ceramic cores are used to form the inner cavity. This will inevitably lead to contact interface reaction between the alloy melt and the ceramic core at high temperature during the solidification process after remelting and pouring of the superalloy. If the interface reaction is serious, t...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22D27/04B22D25/06B22D21/06G01N1/28
Inventor 郑亮杨海青唐定中韩波顾国红
Owner GUIYANG AVIC POWER PRECISION CASTING
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