Integrated alkali metal carrier dynamic desorption device

An alkali metal, integrated technology, applied in the field of chemical applications, can solve the problems of changes in physical and chemical properties, great threat to personnel and property safety, easy oxidation, etc., to prevent oxidation and improve the quality of desorption.

Inactive Publication Date: 2012-05-09
西安航科等离子体科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the active chemical properties of alkali metals, it is easy to oxidize, burn or even explode. Research and testing directly in the air environment poses a greater threat to the safety of personnel and property. At the same time, the oxidation of materials will cause changes in their physical and chemical properties and affect the use effect.

Method used

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  • Integrated alkali metal carrier dynamic desorption device
  • Integrated alkali metal carrier dynamic desorption device

Examples

Experimental program
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Embodiment

[0029] The composition of the integrated alkali metal carrier dynamic desorption device includes: the vacuum chamber 3 is divided into upper and lower sections, the upper section is a hot zone vacuum chamber, and the lower section is a cold zone vacuum chamber; Coil) 9, the inner side is a cavity for heating the alkali metal carrier 10; the vacuum chamber in the cold zone and the sealing flange 2 form a sealed cabin through O-rings and bolts; the sealing flange 2 is provided with a vacuum valve 1, a condensation pipe 12 interface and signal line interface; the current collector 7 is combined with the upper section through threads in the vacuum chamber 3, and supports the alkali metal carrier to the heating area of ​​the resistance furnace 9 through the support frame 8; the drainage tube under the current collector 7 A condenser 11 is installed outside; the collection cup 5 in the vacuum chamber 3 is placed on the load cell 4, and the load cell 4 is connected to the display reco...

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PUM

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Abstract

The invention relates to an integrated alkali metal carrier dynamic desorption device, comprising a vacuum chamber, an alkali metal carrier support component, an alkali metal collection component, a monitoring component and a heating component, wherein the vacuum chamber comprises a vacuum valve, a heat-zone vacuum chamber, a cold-zone vacuum chamber and a sealing flange, an open end below the heat-zone vacuum chamber stretches into the cold-zone vacuum chamber, the alkali metal collection component comprises a current collector and a condenser, the alkali metal carrier support component comprises a support frame used for supporting an alkali metal carrier, the monitoring component comprises a weighing device placed on the sealing flange, a collection cup placed on the weighing device and a display recorder arranged outside the vacuum chamber, the collection cup is arranged right below a drainage tube, the weighing device is connected with the display recorder, and the heating component is arranged outside the hot-zone vacuum chamber. The invention provides a simulation test means for researching internal relation between flow rate and flow velocity indexes and conditions such as temperature, pressure, time and the like when alkali metal working medium is desorbed from a carrier.

Description

technical field [0001] The integrated alkali metal carrier dynamic desorption device provided by the invention belongs to the chemical industry application field, and is especially used in the research and test of the alkali metal desorption performance. Background technique [0002] The alkali metal adsorbed in the capillary carrier is stored in the carrier in a relatively stable form under the action of van der Waals force and chemical bond force. In order to restore it before application, it needs to be separated from the adsorption interface during desorption, and it needs to be detached from the capillary structure by certain means. At home and abroad, there are many studies on the adsorption and desorption of activated carbon porous materials on various pollutants, but there are few reports on the research technology on the desorption performance of alkali metals in porous metal carriers. Because the physical and chemical properties of activated carbon and alkali meta...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N33/20
Inventor 王浩静王红飞杨丽清王晶宇何美林
Owner 西安航科等离子体科技有限公司
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