Preparation method and quality control method of wild chrysanthemum flower compound granule

A technology of wild chrysanthemum and granules, which is applied in the direction of pharmaceutical formulas, medical preparations containing active ingredients, and bulk transportation, and can solve problems such as new preparations of compound granules that have not been seen.

Inactive Publication Date: 2012-10-10
郁建平
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] At present, there are no reports of new compound granule preparations with wild chrysanthemums, grass corals and snake grapes as the main drugs in China

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Example 1: Preparation of wild chrysanthemum compound granules

[0028] Take 100 kg of wild chrysanthemum medicinal materials and 70 kg of grass coral medicinal materials, roughly crush them through a 20-mesh sieve, add 2500 kg of water, and extract for 0.4 hours, add 50 kg of Snake Snake grapes, boil for 0.1 hour, filter the dregs and add 1700 kg of water to extract For 0.1 hour, filter, combine the filtrate, membrane filter, concentrate under reduced pressure to a relative density of 1.05-1.15, and spray-dry the concentrate to obtain compound wild chrysanthemum spray-dried powder; add 0-5 parts of its own weight to the compound wild chrysanthemum spray-dried powder % Of the excipient dextrin is dry granulated to obtain wild chrysanthemum compound granules.

Embodiment 2

[0029] Example 2: Wild Chrysanthemum Compound Granules

[0030] Take 100 kg of wild chrysanthemum medicinal materials and 70 kg of grass coral medicinal materials, roughly crush them through a 20-mesh sieve, add 2500 kg of water, and extract for 0.4 hours, add 50 kg of Snake Snake grapes, boil for 0.1 hour, filter the dregs and add 1700 kg of water to extract After 0.1 hour, filter, combine the filtrate, membrane filter, concentrate under reduced pressure to a relative density of 1.15, and vacuum dry to obtain compound wild chrysanthemum vacuum drying powder; add 0-5% of its own weight of auxiliary material paste to compound wild chrysanthemum vacuum drying powder Granulated by refined dry method to obtain compound granules of wild chrysanthemum.

Embodiment 3

[0031] Example 3: Compound Granules of Wild Chrysanthemum

[0032] Take 100 kg of wild chrysanthemum medicinal materials and 70 kg of grass coral medicinal materials, roughly crush them through a 20-mesh sieve, add 2500 kg of water, and extract for 0.4 hours, add 50 kg of Snake Snake grapes, boil for 0.1 hour, filter the dregs and add 1700 kg of water to extract For 0.1 hour, filter, combine the filtrate, membrane filter, concentrate under reduced pressure to a relative density of 1.15, and dry by microwave to obtain compound wild chrysanthemum microwave drying powder; add 0-5% of its own weight of auxiliary material paste to the compound wild chrysanthemum microwave drying powder Granulated by refined dry method to obtain compound granules of wild chrysanthemum.

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PUM

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Abstract

The invention discloses a wild chrysanthemum flower compound granule which is fine in curative effect, stable in quality and convenient to use, and further discloses a formula, a preparation method and a quality control method of the wild chrysanthemum flower compound granule. The wild chrysanthemum flower compound granule is prepared with wild chrysanthemum flowers, sarcandra glabra and ampelopsis grossedentata serving as raw materials. The weight ratio of the wild chrysanthemum flowers to the sarcandra glabra to the ampelopsis grossedentata is 3-10:2-8:1-7. Medicinal materials are extracted by boiling water for 2-3 times, and the wild chrysanthemum flower compound granule is prepared by the technical processes of filtration, depressurization, concentration, membrane filtration, vacuum drying or spray drying or microwave drying, one-step granulation and the like. The content of total flavone of the granule reaches more than 25%.

Description

[0001] The invention relates to a preparation and quality control method of traditional Chinese medicine compound granules, in particular to a preparation and quality control method of wild chrysanthemum compound granules. [0002] Instructions A method for the preparation and quality control of wild chrysanthemum compound granules. Background technique [0003] Traditional Chinese medicine compound granules are processed under the guidance of the theory of traditional Chinese medicine through various processes of raw materials of Chinese medicinal materials. Carry; the product process and quality standards of traditional Chinese medicine compound granules are not uniform in China. At present, most of the traditional Chinese medicine compound granules are extracted with water, or extracted with water after extracting volatile oil. Different production units have different equipment and processes, resulting in product quality of different manufacturers. Inconsistent, there are...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/87A61K9/16A61P1/00A61P11/00A61P31/04
Inventor 郁建平郁建生郁浩翔
Owner 郁建平
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