Nitrobenzene full-simulation explosive simulant
An explosive simulant, nitrobenzene technology, applied in the direction of aromatic nitration composition, etc., can solve the problems of inability to achieve full simulation, element composition, element percentage content and color difference, affecting the accuracy of the material identified by the security detector, etc. The effect of reducing insecurity
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Embodiment 1
[0028] Take a 300ml clean Erlenmeyer flask, put it into a magnet for stirring, first add 19.27g of accurately measured lactic acid, start stirring, adjust the stirring speed to 600r / min, and add 55.93g of 2,4-toluene diisocyanate while stirring; Turn on the temperature rise, and when the temperature rises to 50°C, keep the constant temperature and add 24.80g of phthalimide; after the addition is completed, adjust the stirring speed to 800r / min, and continue stirring for 30min to completely dissolve the phthalimide, and cool to After room temperature, the material is discharged to obtain a liquid simulant of nitrobenzene. The determined element percentage content is: C 59.01%, H 4.05%, O 25.68%, N 11.26%, the error is within ± 2%, and its atomic number is calculated to be equal to that of nitrobenzene. Compared with nitrobenzene, the atomic number The ordinal number is equal, the color and appearance are the same, and the element percentage is within the error range, which is c...
Embodiment 2
[0030] Take a 300ml clean Erlenmeyer flask, put it into a magnet for stirring, first add 22.94g of dimethyl malonate accurately measured, start stirring, adjust the stirring speed to 600r / min, add 70.61g of 2,4-toluene diisocyanate; add After the completion, start the temperature rise. When the temperature rises to 80°C, add (p)benzoquinone 6.45g at a constant temperature. After the addition, adjust the stirring speed to 800r / min, and continue stirring for 30min to completely dissolve the solid matter. Cool to room temperature and discharge , to obtain liquid simulants of nitrobenzene. The determined element percentage content is: C 58.84%, H 4.12%, O 25.72%, N 11.32%, the error is within ± 2%, and its atomic number is calculated to be equal to that of nitrobenzene. Compared with nitrobenzene, the atomic number The ordinal number is equal, the color and appearance are the same, and the element percentage is within the error range, which is consistent with nitrobenzene.
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