Method for weaving net composite catalytic material from nanometer titania and polytetrafluoroethylene in mixing manner, and application of net composite catalytic material
A technology of nano-titanium dioxide and polytetrafluoroethylene, applied in the direction of organic compound/hydride/coordination complex catalysts, chemical instruments and methods, physical/chemical process catalysts, etc., can solve the problem of photocatalytic performance, poor photocatalytic performance, high cost
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[0020] The method for weaving nano-titanium dioxide and polytetrafluoroethylene into a mesh-like composite catalytic material in the present invention directly uses ball milling to load nano-titanium dioxide on the polytetrafluoroethylene, and has the characteristics of adjustable density, including the following steps:
[0021] 1) Place the polytetrafluoroethylene cylinder in a cylindrical ball mill jar;
[0022] 2) Place the grinding ball and the titanium dioxide powder in the ratio of (10-30):1 in the polytetrafluoroethylene cylinder cavity;
[0023] 3) Adjusting the rotational speed of the ball mill and the ball milling time to obtain a mesh-shaped nano-titanium dioxide-polytetrafluoroethylene composite catalytic material.
[0024] The above-mentioned grinding balls are agate balls or zirconia balls.
[0025] The outer diameter of the polytetrafluoroethylene cylinder in the above step 1) is the same as the inner diameter of the cylindrical ball milling jar, and the radial...
Embodiment 1
[0036] Put the cylindrical polytetrafluoroethylene with a radial thickness of 10mm in a cylindrical ball milling tank with an inner diameter of 100mm (that is, the outer diameter of the cylindrical polytetrafluoroethylene is 100mm and the inner diameter is 80mm), and the cylindrical ball mill The volume of the tank is 500ml, and 50g of agate balls and 5g of TiO with an average particle size of 2μm are mixed according to the ball-to-material ratio of 10:1. 2 The powder is placed in the cavity of a cylindrical polytetrafluoroethylene. Adjust the rotating speed of the ball mill to 400rpm. After 10 hours of ball milling, the mesh-shaped nano-TiO can be obtained 2 - Polytetrafluoroethylene compound. Nano-TiO in its mesh-like composite 2 The average particle size is 500nm, the flake size is 3.6mm, and the density is 1.20g / cm 3 .
Embodiment 2
[0038] A cylindrical polytetrafluoroethylene with a radial thickness of 20mm is placed in a cylindrical ball milling jar with an inner diameter of 300mm. The volume of the cylindrical ball milling jar is 1000ml, and 120g of zirconia balls and 12g of TiO with an average particle size of 0.8 μm 2 The powder is placed in a cavity of polytetrafluoroethylene. Adjust the rotating speed of the ball mill to 500rpm. After 50 hours of ball milling, the mesh-like nano-TiO can be obtained 2 - Polytetrafluoroethylene compound. Nano-TiO in its mesh-like composite 2 The average particle size is 245nm, the flake size is 5mm, and the density is 0.91g / cm 3 .
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