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Method for measuring diallyl phthalate migration in food contact materials

A technology for diallyl phthalate and food contact materials, which is used in material separation, analysis materials, measuring devices, etc., can solve the problem of low limit of diallyl phthalate and the inability of ordinary instruments to meet the detection requirements, etc. problem, to achieve the effect of strong practicability, accurate and reliable quantification, and good reproducibility.

Active Publication Date: 2013-12-04
常州进出口工业及消费品安全检测中心
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AI Technical Summary

Problems solved by technology

There have been many reports on the detection and research reports [1-4] and detection standards [5-7] of phthalates, but due to the extremely low limit of diallyl phthalate, ordinary instruments cannot meet the relevant requirements. Testing requirements, there is currently no testing method and standard for the migration of diallyl phthalate, so it is urgent to formulate a standard testing method for the migration of phthalates in food simulants to strengthen inspection and supervision

Method used

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  • Method for measuring diallyl phthalate migration in food contact materials
  • Method for measuring diallyl phthalate migration in food contact materials
  • Method for measuring diallyl phthalate migration in food contact materials

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Embodiment Construction

[0017] The food simulants involved in this embodiment include: water, 3% (W / V) acetic acid solution, 4% (V / V) acetic acid solution, 10% (V / V) ethanol solution, and olive oil.

[0018] The method for determining the migration of diallyl phthalate in food contact materials includes the following steps:

[0019] Step 1: Prepare standard working solution, food simulant test solution and blank test solution: the standard working solution is six concentrations of water-based standard working solution prepared from diallyl phthalate and six concentrations of olive Oil standard working solution; food simulant test solution is obtained from food contact materials and food simulants through migration experiments according to the test conditions of GB / T23296.1-2009, including water-based food simulant test solution and olive oil simulant test solution; The blank test solution is a food simulant that has not been in contact with food contact materials;

[0020]The preparation method of t...

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Abstract

The invention discloses a method for measuring diallyl phthalate migration in food contact materials. The method includes the steps: firstly, preparing a standard working solution, a food stimulant test solution and a blank test solution; secondly, adopting a high performance liquid chromatograph-tandem triple quadrupole mass spectrometer to perform liquid chromatograph-tandem mass spectrum measurement on the three solutions in the first step, drawing a regression curve of the standard working solution by taking concentration x of phthalate in the standard working solution as an abscissa and corresponding measured quantitative ion peak area y as an ordinate, and calculating slope a and intercept b of the regression curve according to a linear equation, of y=ax+b, obtained by the curve; thirdly, according a formula that c=[(y-y)-b] / a, calculating concentration of diallyl phthalate in the food stimulant test solution. By the aid of the method, migration of the diallyl phthalate in the food contact materials can be measured accurately, quantification is accurate and reliable, and reproducibility is good.

Description

technical field [0001] The invention relates to a method for measuring the migration of diallyl phthalate in food contact materials. Background technique [0002] Phthalates are the most common plasticizers in the plastics industry. They are widely added to the production of polymer plastic products and are widely used in many materials such as toys, food packaging materials, medical blood bags and hoses, wallpapers, etc. . Phthalate esters are announced by the World Health Organization as an environmental hormone, which has the effect of estrogen and will interfere with the human endocrine system in the body. Many foods in daily life may cause phthalates to dissolve and penetrate into the food during processing, heating, packaging, and packaging. The Taiwan beverage incident in 2011 and the Jiuguijiu plasticizer health and safety incident in 2012 made phthalates and related food packaging safety issues a field of high public concern. [0003] Diallyl phthalate is a react...

Claims

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Application Information

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IPC IPC(8): G01N30/02G01N30/06
Inventor 罗世鹏徐炎商贵芹吴泽颖刘君峰王红松
Owner 常州进出口工业及消费品安全检测中心
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