A kind of preparation method of medium permittivity microwave dielectric ceramic material
A technology of microwave dielectric ceramics and electrical constants, which is applied in the field of low-temperature co-fired ceramic powder preparation, which can solve the problems of large sintering shrinkage, high preparation cost, and high mechanical strength, and achieve low sintering temperature and low production cost. , the effect of short production cycle
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Embodiment 1
[0028] Weigh 80gCa(OH) 2 , 10gLi 2 CO 3 , 100gNb 2 o 5 , 10gTiO 2 Mix, add 160g of deionized water and 400g of zirconia balls, and use wet ball milling for 10 hours; filter the ball-milled mixture, dry it at 120°C, and pre-fire it at 860°C, and grind it into 250μm green ceramic powder particles ;
[0029] Weigh 84.45gH 3 BO 3 , 15.55g ZnO, add 80g deionized water and 200g zirconia balls, use wet ball milling for 8 hours, filter the mixture after ball milling, dry at 110°C, then quench in molten water at 1500°C, and grind into 200μm Green porcelain powder particles;
[0030] Weigh 99g of raw porcelain powder and 1g of glass powder, add 50g of absolute ethanol and 200g of zirconia balls, and use wet ball milling for 12 hours; add 30ml of 5% PVB polymer binder aqueous solution, ball mill for 6 hours, mix evenly, and make The pellets are pressed into tablets; the pressed ceramic pieces are heated in a kiln-type sintering furnace at a heating rate of 2 °C / min to 500 °C for...
Embodiment 2
[0032] Weigh 86.6gCa(OH) 2 , 10.4gLi 2 CO 3 , 90.4gNb 2 o 5 , 12.6gTiO 2 Mix, add 160g of deionized water and 400g of zirconia balls, and use wet ball milling for 12 hours; filter the ball-milled mixture, dry it at 100°C, and then pre-fire it at 830°C, and grind it into 200μm green ceramic powder particles ;
[0033] Weigh 80.25gH 3 BO 3 , 19.75g ZnO, add 80g deionized water and 200g zirconia balls, use wet ball milling for 10 hours, filter the mixture after ball milling, dry at 105°C, then quench in molten water at 1450°C, and grind into 220μm Green porcelain powder particles;
[0034]Weigh 98g of raw porcelain powder and 2g of glass powder, add 50g of absolute ethanol and 200g of zirconia balls, and use wet ball milling for 10 hours; add 20ml of 15% PVA polymer binder aqueous solution, ball mill for 5 hours, mix evenly, and make The pellets are pressed into tablets; the pressed ceramic pieces are heated in a kiln-type sintering furnace at a heating rate of 2°C / min t...
Embodiment 3
[0036] Weigh 91gCa(OH) 2 , 13gLi 2 CO 3 , 83gNb 2 o 5 , 13gTiO 2 Mix, add 160g of deionized water and 400g of zirconia balls, and use wet ball milling for 10 hours; filter the ball-milled mixture, dry it at 120°C, and then pre-fire it at 850°C, and grind it into 280μm green ceramic powder particles ;
[0037] Weigh 78.45gH 3 BO 3 , 21.25g ZnO, add 80g deionized water and 200g zirconia balls, use wet ball milling for 9 hours, filter the mixture after ball milling, dry at 100°C, then quench in molten water at 1400°C, and grind into 260μm Green porcelain powder particles;
[0038] Weigh 97g of raw porcelain powder and 3g of glass powder, add 50g of absolute ethanol and 200g of zirconia balls, and use wet ball milling for 12 hours; add 40ml of 10% PVA polymer binder aqueous solution, ball mill for 4 hours, mix evenly, and make The pellets are pressed into tablets; the pressed ceramic pieces are heated in a kiln-type sintering furnace at a heating rate of 2°C / min to 500°C ...
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