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Production process of preparing white carbon black from rice husk ash

A production process and technology of rice husk ash, applied in the field of production technology for preparing white carbon black, can solve the problems of low product whiteness and purity, simple and extensive production process, large energy consumption in the production process, etc. Whiteness, good quality, the effect of reducing the content

Active Publication Date: 2015-08-19
QUECHEN SILICON CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] In the traditional process, because the production process is simple and extensive, the production process consumes a lot of energy, the impurity content is high, and the product whiteness and purity are not high, but there are many factors that affect the product characteristics, and the factors interact with each other. To ensure a good Product quality urgently needs to explore new technological means, improve traditional technological methods, and improve product quality

Method used

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  • Production process of preparing white carbon black from rice husk ash

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] Utilize rice husk ash to prepare the production technology of white carbon black, concrete process steps are as follows:

[0041] A. Pretreatment of rice husk ash:

[0042] After removing impurities, the rice husk ash was crushed to 100 meshes, water 11 times its mass was added to the rice husk ash, and a compound chelating agent a with a mass of 0.34% of the rice husk ash was added, soaked at 40°C for 3 hours, then centrifuged and washed with water. Dry at 500°C to obtain the pretreated rice husk ash for subsequent use;

[0043] Wherein the complex chelating agent a is made up of aminotriacetic acid, N-carboxyethylethylenediaminetriacetic acid, aminotrimethylene phosphonic acid, and the mass ratio of each component is, aminotriacetic acid: N-carboxyethylethylenediaminetriacetic acid Acetic acid: amino trimethylene phosphonic acid = 2.6: 1.2: 0.7;

[0044] B, the preparation of water glass:

[0045] Reaction principle: SiO 2 +NaOH→Na 2 O. SiO 2 +H 2 o

[0046]Mi...

Embodiment 2

[0060] Utilize rice husk ash to prepare the production technology of white carbon black, concrete process steps are as follows:

[0061] A. Pretreatment of rice husk ash:

[0062] After removing impurities, the rice husk ash was crushed to 100 meshes, water 8 times its mass was added to the rice husk ash, and a compound chelating agent a with a mass of 0.3% of the rice husk ash was added, soaked at 35°C for 2 hours, then centrifuged and washed with water. Dry at 400°C to obtain the pretreated rice husk ash for subsequent use;

[0063] Wherein the complex chelating agent a is made up of aminotriacetic acid, N-carboxyethylethylenediaminetriacetic acid, aminotrimethylene phosphonic acid, and the mass ratio of each component is, aminotriacetic acid: N-carboxyethylethylenediaminetriacetic acid Acetic acid:amino trimethylene phosphonic acid=2:1:0.5;

[0064] B, the preparation of water glass:

[0065] Reaction principle: SiO 2 +NaOH→Na 2 O. SiO 2 +H 2 o

[0066] Mix the pret...

Embodiment 3

[0080] Utilize rice husk ash to prepare the production technology of white carbon black, concrete process steps are as follows:

[0081] A. Pretreatment of rice husk ash:

[0082] After removing impurities, the rice husk ash was crushed to 100 meshes, water 13 times its mass was added to the rice husk ash, and a compound chelating agent a with 0.4% of the mass of the rice husk ash was added, soaked at 50°C for 4 hours, then centrifuged and washed with water, Dried at 550°C to obtain the pretreated rice husk ash for subsequent use;

[0083] Wherein the complex chelating agent a is made up of aminotriacetic acid, N-carboxyethylethylenediaminetriacetic acid, aminotrimethylene phosphonic acid, and the mass ratio of each component is, aminotriacetic acid: N-carboxyethylethylenediaminetriacetic acid Acetic acid: amino trimethylene phosphonic acid = 3: 1.5: 1;

[0084] B, the preparation of water glass:

[0085] Reaction principle: SiO 2 +NaOH→Na 2 O. SiO 2 +H 2 o

[0086] Mi...

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Abstract

The invention discloses a production process for preparing white carbon black by use of rice hull ash. The process comprises the following steps: pretreating the rice hull ash, reacting the pretreated rice hull ash with an alkaline liquid to generate water glass, aging the water glass and then reacting the aged water glass with an acid to generate the white carbon black. The process is rigorous and scientific, energy-saving and environment-friendly due to recycling of heat, high in finished product purity, high in whiteness, and excellent in stability.

Description

Technical field [0001] The present invention involves the field of chemical industry, and specifically involves the use of rice shells to prepare white charcoal and black production technology. Background technique [0002] The rice shell ash is mainly derived from the burning and thermal solution of the rice shell? According to statistics, the annual output of China's current rice has exceeded 180 million tons, accounting for about one -third of the global annual output.During the processing process, there will be a large amount of rice shells. Can rice shells of about 200kg of rice per ton? These rice shells have caused great inconvenience to transportation due to their natural accumulation density (about 120kg / m3)?On the other hand, most of the rice processing companies do not use a reasonable and effective process to use the rice shells, so many rice shells are used as agriculture [0003] The waste was discarded. [0004] According to statistics, my country's annual rice she...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B33/12
Inventor 宣全
Owner QUECHEN SILICON CHEM