Emulsion for killing aphids and red spiders and preparation method thereof

A red spider and emulsion technology, applied in the field of natural plant applications, can solve the problems of interference of total alkaloid insecticidal activity, poor persistence, difference in insecticidal activity, etc., achieve no environmental pollution, reduce toxicity and irritation, and reduce production costs low effect

Active Publication Date: 2016-02-24
蚌埠圣丹生物化工有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The results of the field efficacy test show that the two extracts of garlic and tea seed cake have a certain control effect on red spider mites, but their persistence is poor (Ningbo Agricultural Science and Technology, 2011, 2: 13-15)
Zhao Botao and others carried out the optimization of the extraction process of the total alkaloids of Sophora flavescens and the research on the aphidicidal activity. The test of the insecticidal activity of the extract of Sophora flavescens on aphids showed that the insecticidal activity of different treatments of Sophora flavescens extract and different extraction solvents The difference is significant; with chloroform as the extraction solvent, the total alkaloid content of the obtained Sophora flavescens is the highest, and its insecticidal activity is the highest; with ethanol as the extraction solvent, the chloroform extract is compared with the concentrated solution, and the chloroform extract has no effect on the total alkaloids at the same concentration. The insecticidal activity of aphids is relatively high, which may be due to the large amount of impurities contained in the ethanol concentrate, which interferes with the insecticidal activity of the total alkaloids (China Wild Plant Resources, 2008, 27(1): 43-46)

Method used

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  • Emulsion for killing aphids and red spiders and preparation method thereof
  • Emulsion for killing aphids and red spiders and preparation method thereof
  • Emulsion for killing aphids and red spiders and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Mix Ailanthus leaf water extract, Sophora flavescens alcohol extract, Eucommia leaf water extract, Neem bark alcohol extract in a weight ratio of 1:1:2:2 to obtain 2.0 g of mixed extract, add n-hexane medium (or xylene, cyclohexanone, cyclohexanol, 200# solvent oil), heat and dissolve at 40°C to obtain a medicinal solution; add emulsifier Tween 80 and auxiliary agent sodium carboxymethylcellulose according to the amount of prescription 1 Add it into the prepared medicinal solution, use ultrasonic emulsification device, ultrasonic frequency is 15kHz, ultrasonic time is 30min, temperature is 60°C to obtain colostrum; slowly add 5% g / mL ethylparaben dropwise to colostrum , 5% g / mL ethylene glycol solution and deionized water at a rate of 3mL / min, heated in a water bath at 60°C, and stirred at 7000r / min at the same time, and continued to stir for 30min after the deionized water was added dropwise. After the emulsion was formed, The temperature should be lowered slowly, and ...

Embodiment 2

[0043] Mix Ailanthus leaf water extract, Sophora flavescens alcohol extract, Eucommia leaf water extract, Neem bark alcohol extract in a weight ratio of 1:1:2:2 to obtain 2.0 g of mixed extract, add n-hexane In the solvent, heat and dissolve at 40°C to obtain a drug solution; add the emulsifier Tween 60 (or Tween 80) and the auxiliary agent carboxymethylcellulose sodium to the prepared drug solution according to the amount of prescription 2, and use ultrasonic emulsification device, the ultrasonic frequency is 15kHz, the ultrasonic time is 30min, and the temperature is 60°C to obtain colostrum; slowly add 5% g / mL ethylparaben and 5% g / mL ethylene glycol solution dropwise to the colostrum and deionized water at a rate of 3mL / min, heated in a water bath at 60°C, and stirred at 7000r / min at the same time, and continued to stir for 30min after adding the deionized water dropwise. The droplets aggregate to give a light yellow emulsion that kills aphids and spider mites.

[0044] Z...

Embodiment 3

[0051] Pesticide Emulsion I was prepared according to the following recipe:

[0052]

[0053] II: Take 1mL of 75% dichlorvos emulsifiable concentrate into a 2000mL large container, add distilled water to dilute to 1500mL;

[0054] III: Take 48% omethoate EC 1mL to a 2000mL large container, add distilled water to dilute to 1500mL;

[0055] IV: clear water.

[0056] Do the control effect test of three seasons continuously, do three times in parallel in each season, investigate the control effect of pesticide emulsion (I), dichlorvos (II) and omethoate (III) of the present invention to aphids, spider mites. The experimental results are shown in Tables 3 and 4:

[0057] The control effect of table 33 kinds of insecticides on aphids

[0058]

[0059] The control effect of table 43 kinds of insecticides to spider mite

[0060]

[0061] in:

[0062]

[0063]

[0064] Tests show that: the pesticide emulsion of the present invention has better control effects on aph...

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Abstract

The invention discloses emulsion for killing aphid and red spider and its preparation method. The emulsion uses mixed extractum as a main medicine, the mixed extractum comprises ailanthus altissima leaf water extraction extractum, radix sophorae flavescentis alcohol extraction extractum, eucommia ulmoides leaf water extraction extractum and neem bark alcohol extraction extractum with a weight ratio of 1:1:2:2, the emulsion also comprises, in relative to each gram of the main medicine, the following components: 40-50mL of a solvent, 5-15mL of an emulsifier, 0.05-0.15g of an assistant, 1-2mL of a preservative, 5-7.5mL of an antifreeze and 50-100mL of deionized water. The preparation method of the emulsion is as follows: (1) mixing the four extraction extractum according to the ratio, adding the solvent, heating for dissolving to obtain a medicine liquid; (2) adding the emulsifier and the assistant to the medicine liquid, using an ultrasonic emulsification device to obtain primary emulsion; (3) successively adding the preservative, the antifreeze and the deionized water to the primary emulsion, stirring, cooling to room temperature to obtain the emulsion. The emulsion is environmental friendly, stable in quality and good in insecticidal effect, and the preparation method has the advantages of simple operation and ow production cost.

Description

technical field [0001] The invention relates to an emulsion for killing aphids and red spiders and a preparation method thereof, belonging to the technical field of natural plant application. Background technique [0002] The world today is facing four major problems, namely population, food, energy and environment. There are more than 1,500 major crop pests and diseases in my country, and dozens of them are particularly serious. So far, chemical control is still the most important means and measures in the management of pests in my country. Among them, more than 95% use chemical pesticides, the proportion of biological pesticides is only 2% to 3%, and emulsions are very few. On the one hand, pesticides play a very important role in killing and inhibiting pests and diseases, and ensuring stable and high yields of crops. At the same time, due to unreasonable use, they will endanger the safety of the environment and human health through various means. There are many highly ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A01N65/26A01N25/04A01P7/02A01P7/04
Inventor 霍清杨晓芳
Owner 蚌埠圣丹生物化工有限公司
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