Constant-temperature double-layer natural essential oil bacteriostatic agent and preparation method thereof
A technology of natural essential oils and antibacterial agents, applied in the field of phytochemistry, can solve the problems of natural essential oils such as easy volatilization and short service life, and achieve the effects of not being volatile, inhibiting deterioration and corruption, and inhibiting the growth of bacteria
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Embodiment 1
[0063] The parts by weight of the prepared raw materials are 4.5 parts of urea, 15 parts of formaldehyde, and 2.2 parts of melamine, and in a three-hole flask connected with a reflux device and a constant temperature magnetic stirrer, a formaldehyde solution with a mass fraction of 37% is added, adjusted with triethanolamine. Its pH value is 7.0~7.5, add 4.5 parts of 95% urea and melamine to the formaldehyde solution, and add deionized water to 60mL, adjust the pH value to 8.5 with triethanolamine, at a constant temperature of 70 ° C, stirring speed 400r / urea-formaldehyde resin prepolymer was obtained by reacting for 1 h under the condition of min; weighed 20 parts of n-tetradecane as the core material, 0.45 parts of Span-80, 0.55 parts of Tween-80, and 40 parts of deionized water. Homogenously emulsify n-tetradecane, Span-80, Tween-80 and deionized water under the action of a high-shear dispersing emulsifier to obtain a uniform organic phase change material emulsion; weigh th...
Embodiment 2
[0066] The parts by weight of the prepared raw materials are 5.0 parts of urea, 18 parts of formaldehyde, and 2.5 parts of melamine, and in a three-hole flask connected with a reflux device and a constant temperature magnetic stirrer, a formaldehyde solution with a mass fraction of 37% is added, adjusted with triethanolamine. Its pH value is 7.0~7.5, add 5.0 parts of 95% urea and melamine to the formaldehyde solution, and add deionized water to 60mL, adjust the pH value to 8.5 with triethanolamine, at a constant temperature of 70°C and a stirring speed of 400r / urea-formaldehyde resin prepolymer was obtained by reacting for 1 h under the condition of min; weighed 25 parts of n-tetradecane as the core material, 0.48 parts of Span-80, 0.52 parts of Tween-80, and 45 parts of deionized water. Homogenously emulsify n-tetradecane, Span-80, Tween-80 and deionized water under the action of a high-shear dispersing emulsifier to obtain a uniform organic phase change material emulsion; we...
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