High heat absorption high-brightness bottle-grade polyester chip and preparation method thereof
A technology of polyester chips and high brightness is applied in the field of high-endothermic and high-brightness bottle-grade polyester chips and their preparation. , The effect of good crack resistance and low acetaldehyde content
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example 1
[0026] (1), mix titanium nitride with ethylene glycol, and prepare a titanium nitride mixed solution with a titanium nitride concentration of 1% by weight; mix barium sulfate with ethylene glycol, and prepare a mixed solution of barium sulfate with 0.5% by weight ;
[0027] (2), esterification reaction:
[0028] After mixing terephthalic acid (PTA), ethylene glycol (EG), antimony acetate, and toner into slurry, it enters the esterification kettle. The esterification reaction temperature is 270°C, the reaction pressure is 0.3 Mpa, and the reaction time is 2.5 hours; the weight ratio of terephthalic acid and ethylene glycol is 4:1; the amount of antimony acetate added is 550ppm in the weight content of the finished polyester chips; the toner is composed of redness agent and blueness agent, redness The additive amount is that the weight content in the finished polyester is 0.4ppm, and the blueness agent additive amount is that the weight content in the finished polyester is 0.6p...
example 2
[0037] (1), mix titanium nitride with ethylene glycol, and prepare a titanium nitride mixed solution with a titanium nitride concentration of 1% by weight; mix barium sulfate with ethylene glycol, and prepare a mixed solution of barium sulfate with 0.5% by weight ;
[0038] (2), esterification reaction:
[0039] After mixing terephthalic acid (PTA), ethylene glycol (EG), antimony acetate, and toner into slurry, it enters the esterification kettle. The esterification reaction temperature is 270°C, the reaction pressure is 0.3 Mpa, and the reaction time is 2.5 hours; the weight ratio of terephthalic acid and ethylene glycol is 4:1; the amount of antimony acetate added is 550ppm in the weight content of the finished polyester chips; the toner is composed of redness agent and blueness agent, redness The additive amount is that the weight content in the finished polyester is 0.4ppm, and the blueness agent additive amount is that the weight content in the finished polyester is 0.6p...
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