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A graphite component purification device

A technology for purifying devices and components, applied in the directions of graphite, inorganic chemistry, carbon compounds, etc., can solve the problems of long cycle and dangerous operation, and achieve the effect of purifying graphite components and ensuring purity

Active Publication Date: 2015-09-02
青海黄河上游水电开发有限责任公司新能源分公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There is a certain degree of operational risk in the operation of this method, and it takes a certain amount of time to cool down after high-temperature calcination, and the cycle is longer

Method used

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  • A graphite component purification device
  • A graphite component purification device

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Embodiment Construction

[0020] Such as figure 1 , figure 2 Shown, a kind of graphite parts purifying device, this device comprises is provided with the shell 4 that is cylindrical and is provided with base, places the airtight door 11 of shell 4 side, places the cavity in shell 4 and places in the cavity The support 6 for placing graphite parts 7. Three electrodes 1 with cooling water jackets connected to the power supply are evenly distributed on the shell 4, the upper part is provided with an exhaust pipe port 9, and the bottom is provided with an air intake pipe port 10; the shell 4 and the cavity are connected. Heat-insulating graphite mesh 5; three graphite electrodes 8 are arranged between the cavity and the bracket 6, and the three graphite electrodes 8 are connected to the three electrodes 1 with cooling water jackets one by one; the exhaust pipe port 9 is connected to the vacuum pump Connected; the inlet pipe port 10 is connected with the chlorine tank.

[0021] Wherein: each of the thre...

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Abstract

The invention relates to a graphite part purifying device, comprising a cylindric shell with a pedestal, a hermetic door located at one side of the shell, a cavity located in the shell and a support located in the cavity and used for placing of a graphite part, wherein three electrodes with cooling water jackets are uniformly distributed on the shell and connected with a power supply, the upper part of the shell is provided with a tail gas pipe orifice, the bottom of the shell is provided with an air inlet pipe orifice, a heat insulating graphite net is arranged at the joint of the shell and the cavity, three graphite electrodes are arranged between the cavity and the support and are connected with the three electrodes with the cooling water jackets in the manner of one-to-one correspondence, the tail gas pipe orifice is connected with a vacuum pump, and the air inlet pipe orifice is connected with a chlorine tank. The graphite part purifying device can effectively remove impurities in the graphite part, thereby guaranteeing purity of polysilicon.

Description

technical field [0001] The invention relates to a purification device, in particular to a graphite component purification device. Background technique [0002] The graphite parts used in polysilicon electrodes are all high-purity graphite, but graphite parts will be polluted during the process of manufacturing. The surface and interior of graphite parts will be polluted with metal impurities, boron, phosphorus, arsenic, grease, etc. Elements, boron, phosphorus, arsenic, etc. In the polysilicon production process, graphite parts are in direct contact with polysilicon products, and impurities in graphite parts will enter into polysilicon products, affecting the purity of polysilicon products. [0003] At present, the purification technology of graphite components mainly consists of the following two types: [0004] One is to use strong acid (concentrated nitric acid) to soak, then use pure water to wash and dry. This method uses the oxidizing property of strong acid to oxidi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B33/021C01B31/04C01B32/21C01B32/215
Inventor 刘柏年刘刚李文强刘康斐陈英李春松秦榕
Owner 青海黄河上游水电开发有限责任公司新能源分公司