Supercharge Your Innovation With Domain-Expert AI Agents!

Electrolytic solution for tungsten helix electropolishing and method for tungsten helix electropolishing

An electrolytic polishing and helical technology, applied in the field of electrolyte, can solve the problems of poor heat dissipation of traveling wave tubes, affecting the performance of traveling wave tubes, complex composition of electrolyte, etc., and achieve improved smoothness, strong heat dissipation performance, and polishing precision high effect

Active Publication Date: 2016-07-06
NANJING SANLE GROUP
View PDF1 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The tungsten helix is ​​an important component of the slow wave structure in the traveling wave tube. The smoothness of the surface of the tungsten helix directly affects the performance of the traveling wave tube. If the surface of the traveling wave tube is uneven and has burrs, it will cause the heat dissipation of the traveling wave tube. Poor performance directly affects the performance of the traveling wave tube. The electrolytic polishing method used in the prior art has complex electrolyte composition, poor environmental performance, and unstable polishing process. It is also very high, so in the process of polishing, the requirements for polishing quality are very good. The polishing liquid and polishing process of the prior art cannot meet the working requirements of traveling wave tubes with high power, large working ratio and high precision requirements.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Electrolytic solution for tungsten helix electropolishing and method for tungsten helix electropolishing
  • Electrolytic solution for tungsten helix electropolishing and method for tungsten helix electropolishing
  • Electrolytic solution for tungsten helix electropolishing and method for tungsten helix electropolishing

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0060] 1. An electrolyte for tungsten helix electrolytic polishing, which is made of the following raw materials:

[0061] Na 3 PO 4 120g / L, NaOH8g / L, glycerol 15mL / L, solvent is water.

[0062] 2. A method for electrolytic polishing of a tungsten helix, comprising the following steps:

[0063] (1) Put the tungsten helix into the acetone solution for ultrasonic treatment for 10 minutes;

[0064] (2) Then immerse the tungsten helix in a 1:1 hydrochloric acid solution, and weakly etch it for 0.5-1s;

[0065] (3) Then put the tungsten helix into the concentration of 120g / LNa 3 PO 4 , 8g / LNaOH, glycerol 15mL / L mixed aqueous solution, at 70 ℃, under the condition of polishing voltage 10V, carry out electropolishing treatment for 50s;

[0066] (4) After polishing, immerse the tungsten helix in hydrochloric acid for neutralization;

[0067] (5) Then immerse in chromic acid to remove surface oxides;

[0068] (6) Dehydration and drying.

[0069] Observed under a magnifying gla...

Embodiment 2

[0071] 1, a kind of electrolyte of described tungsten helix electrolytic polishing, it is made of following raw material:

[0072] Na 3 PO 4 100g / L, NaOH6g / L, glycerol 10mL / L, solvent is water.

[0073] 2. A method for electrolytic polishing of a tungsten helix provided by the present invention comprises the following steps:

[0074] (1) Put the tungsten helix into the acetone solution for ultrasonic treatment for 15 minutes; this step can remove the residual oil, dust and other dirt on the surface.

[0075] (2) Then immerse the tungsten helix in a 1:1 hydrochloric acid solution, and weakly etch it for 0.5-1s;

[0076] (3) Then put the tungsten helix into the concentration of 100g / LNa 3 PO 4 , in a mixed aqueous solution of 6g / LNaOH and 10mL / L glycerin, at 50°C and a polishing voltage of 7V, perform electrolytic polishing for 30s;

[0077] (4) After polishing, immerse the tungsten helix in hydrochloric acid for neutralization;

[0078] (5) Then immerse in chromic acid t...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses an electrolyte solution for tungsten helical electrolytic polishing and a polishing method thereof. The polishing solution is made of the following raw materials: Na 3 PO 4 100g / L~120g / L, NaOH 6g / L~8g / L, glycerol 10~15mL / L, solvent is water. The electrolytic solution provided by the invention has scientific and reasonable proportions of components, and has the advantages of non-toxicity, low pollution, low corrosion and the like. The tungsten helical wire electrolytic polishing method described in the present invention has strong operability and good electrolytic polishing effect, and can improve the smoothness of the surface of the tungsten helical wire mesh by one level under the conditions of optimal electrolytic voltage, time, temperature and other process parameters. , The size consumption of the tungsten helix during the polishing process is small, the polishing precision is high, and the quality of the tungsten helix obtained by polishing is high. After being assembled into the traveling wave tube, the heat dissipation performance is strong, which can improve the performance of the traveling wave tube.

Description

technical field [0001] The invention designs an electrolyte, in particular to an electrolyte for tungsten helix electrolytic polishing and a method for electrolytic polishing using the electrolyte. Background technique [0002] The tungsten helix is ​​an important component of the slow wave structure in the traveling wave tube. The smoothness of the surface of the tungsten helix directly affects the performance of the traveling wave tube. If the surface of the traveling wave tube is uneven and has burrs, it will cause the heat dissipation of the traveling wave tube. Poor performance directly affects the performance of the traveling wave tube. The electrolytic polishing method used in the prior art has complex electrolyte composition, poor environmental performance, and unstable polishing process. It is also very high, so in the process of polishing, the requirements for polishing quality are very good. The polishing liquid and polishing process of the prior art cannot meet t...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C25F3/26
Inventor 刘洋高志强郑海鹰邹雯婧孙萌
Owner NANJING SANLE GROUP
Features
  • R&D
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More