Solid base catalyst for preparing biodiesel
A solid base catalyst, biodiesel technology, applied in physical/chemical process catalysts, biofuels, petroleum industry and other directions, can solve the problems of high energy consumption and high equipment requirements, and achieve the effects of easy purification, cost reduction and easy separation
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0022] Weigh 5.7g ZnCl 2 , 16.5g MnCl 2 and 20.7g K 2 CO 3 , respectively dissolved in deionized water to obtain a mass fraction of 5.4% ZnCl 2 Solution, the mass fraction is 14.2% MnCl 2 solution and mass fraction is 3.3% K 2 CO 3 solution.
[0023] At 60°C, the ZnCl 2 solution and MnCl 2 The solution was mixed and poured into K 2 CO 3 solution, and stir rapidly to make the solution fully mixed and precipitated;
[0024] Stand still, cool, and age at room temperature. The precipitate was washed thoroughly with deionized water until the conductivity of the washed-out solution was almost equal to that of deionized water. Filter and dry, then calcinate at 400°C for 24 hours, and obtain manganese carbonate zinc oxide composite solid base catalyst after cooling.
[0025] In a 500ml high-temperature and high-pressure reactor equipped with internal reflux and mechanical stirring, add the above-mentioned solid catalyst, methanol and soybean oil in sequence according to t...
Embodiment 2
[0027] Weigh 8.5g ZnCl 2 , 10g MnCl 2 and 22g K 2 CO 3 , respectively dissolved in deionized water to obtain a mass fraction of 7.8% ZnCl 2 Solution, mass fraction is 11.0% MnCl 2 solution and mass fraction is 3.3% K 2 CO 3 solution.
[0028] At 55°C, the ZnCl 2 solution and MnCl 2 The solution was mixed and poured into K 2 CO 3 solution, and stir rapidly to make the solution fully mixed and precipitated;
[0029] Stand still, cool, and age at room temperature. The precipitate was washed thoroughly with deionized water until the conductivity of the washed-out solution was almost equal to that of deionized water. Filter and dry, then calcinate at 300°C for 0.5h, and cool to obtain a manganese carbonate zinc oxide composite solid base catalyst.
[0030] In a 500ml high-temperature and high-pressure reactor equipped with internal reflux and mechanical stirring, add the above-mentioned solid catalyst, methanol and soybean oil in sequence according to the catalyst mass...
Embodiment 3
[0032]Weigh 8.5g ZnCl 2 , 10g MnCl 2 and 18g K 2 CO 3 , respectively dissolved in deionized water to obtain a mass fraction of 7.8% ZnCl 2 Solution, mass fraction is 11.0% MnCl 2 solution and mass fraction is 3.3% K 2 CO 3 solution.
[0033] At 65°C, the ZnCl 2 solution and MnCl 2 The solution was mixed and poured into K 2 CO 3 solution, and stir rapidly to make the solution fully mixed and precipitated;
[0034] Stand still, cool, and age at room temperature. The precipitate was washed thoroughly with deionized water until the conductivity of the washed-out solution was almost equal to that of deionized water. Filter and dry, then calcinate at 400°C for 24 hours, and obtain manganese carbonate zinc oxide composite solid base catalyst after cooling.
[0035] In a 500ml high-temperature and high-pressure reactor equipped with internal reflux and mechanical stirring, add the above-mentioned solid catalyst, methanol and soybean oil in sequence according to the cataly...
PUM
Login to view more Abstract
Description
Claims
Application Information
Login to view more - R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap