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293results about How to "Easy to refine" patented technology

Synchronous aqueous enzymatic ultrasonic extraction for walnut oil and walnut protein peptide

The invention relates to an enzyme method ultrasonic extraction method of walnut oil and walnut protein, which belongs to the food and the functional food field. Water is added into walnut kernel or walnut powder to be grinded into paste, protease or compound protease are added into to be performed hydrolization, and simultaneously ultrasonic processing is performed, then the walnut kernel or walnut powder is agitated to perform enzymatic extraction, and then centrifugal separation oil phase, protein peptide oil water phase and residual solid phase are performed; walnut oil is acquired by refining the obtained oil phase, which meets the requirements of green foods; the protein peptide aqueous solution can be directly used to produce degreased walnut protein nutrient milk, or to prepare walnut antioxidation peptide after performed nanofiltration, which is used in health products, food additives, cosmetics or daily chemical articles, or to produce nutrient condensed milk after being performed low temperature concentrating, or to produce walnut protein nutrition powder after performed spray drying; the solid phase residue is prepared into diet fiber food after being dried and grinded into powder; walnut nutrient protein peptide products can be obtained through performing vacuum concentration and spray drying to walnut protein peptide extracting solution containing nutrient content.
Owner:KUNMING UNIV OF SCI & TECH

Alloy ingot for automotive hub and production method thereof

The invention discloses an alloy ingot for an automotive hub and a production method thereof. The alloy ingot comprises the following components: 6.8-7.2% of Si, 0.28-033% of Mg, 0.10-0.15% of Ti, 0.015-0.030% of Sr, less than or equal to 0.10% of Fe, less than or equal to 0.05% of Mn, less than 0.01% of zinc, less than 0.01% of Cu, less than 0.003% of Ca, less than 0.002% of P, less than 0.02% of other single impurity content, less than 0.1% of total impurity content and the balance of aluminum. The production method of the alloy ingot for the automotive hub comprises the following steps of: adding 3303 industrial metallic silicon and electrolytic aluminum liquid for batching, heating at an appropriate temperature and melting, spreading a covering agent so as to reduce oxidation slagging, stirring so that the industrial metallic silicon rapidly melts, keeping uniform temperature, slagging off, keeping melt clean, spraying powder and refining by adopting high-purity N2 and a refined powder spraying agent, controlling the temperature of a smelting furnace to 740-750 DEG C, adding Al-Sr alloy to aluminium water, carrying out secondary degassing and slagging-off by adopting a powder spraying refinement method, filtering to remove slag, and casting the alloy ingot in line with requirements. The alloy ingot obtained by the method has the advantages of stable and uniform components, compact structure and clean surface; and the production method is the best production method for producing the A356.2 alloy ingot for the low-iron high-end automotive hub.
Owner:河南省银湖铝业有限责任公司

Method for separating copper, cobalt and manganese from cupric chloride manganese-cobalt-calcium-zinc impurity removal solution

The invention relates to a method for separating copper, cobalt and manganese from a cupric chloride manganese-cobalt-calcium-zinc impurity removal solution. The method comprises the steps that sodium sulfate is added to the cupric chloride manganese-cobalt-calcium-zinc solution, and calcium sulfate is removed by filtration; then sodium carbonate is added to a solution obtained in step one, a pH value is adjusted to 4.0-6.0 to allow copper ions in the solution to be precipitated, and copper precipitates are obtained by filtration separation; the copper precipitates are dissolved with sulfuric acid and are subjected to evaporation crystallization to form copper sulfate crystals; manganese powder is added to a solution after copper removal to allow cobalt ions to be reduced to cobalt powder to be precipitated, and cobalt powder is obtained after the filtration separation and is dissolved with acid to form a cobalt solution; and a solution after cobalt removal contains manganese and a little zinc and calcium, manganese is precipitated through the evaporation crystallization or by adding sodium carbonate, and manganese salts such as rough manganese carbonate are obtained. With the adoption of the method, three main valuable metals, namely copper, cobalt and manganese, can be separated and extracted economically and conveniently.
Owner:长沙百汇新材料科技有限公司

Method for hydrofining caprolactam in magnetically stabilized bed

The invention relates to a method for hydrofining caprolactam in a magnetically stabilized bed. The method comprises the following steps: the acidamide oil is extracted and distilled with benzene/cyclohexane to obtain the caprolactam crude product; in a magnetically stabilized bed reactor, the hydrogenation reaction is carried out under the action of a catalyst formed by active components such as platinum or/and palladium and a magnetic spherical carrier, so that the unsaturated substance in the liquid caprolactam crude product reacts with hydrogen to generate a saturated substance; and then the saturated substance is rectified to obtain the caprolactam product. The active components in the catalyst occupy 0.01-5 percent (wt); and the hydrogenation reaction conditions are as follows: temperature: 80 DEG C to 140 DEG C, pressure: 0.5 to 3.0 MPa, air speed: 2 to 60h-1, and magnetic field intensity: 10 to 1500 oersteds. Compared with the prior art, the method has the advantages that the procedures of water re-extraction and dehydration by evaporation are reduced, the refining process is greatly simplified, and the refining operation process is optimized; and the method is favorable for reducing energy consumption and environmental pollution and enhancing the processing capacity of the device.
Owner:CHINA PETROLEUM & CHEM CORP +3

High-strength and high-conductivity rare earth copper alloy for contact lines and preparation method thereof

The invention relates to a high-strength and high-conductivity rare earth copper alloy for contact lines and a preparation method thereof. The rare earth copper alloy is composed of chromium, zirconium, zinc, titanium, silver, copper, rare earth elements and inevitable impurity elements, wherein during preparation, a Cu-Zr intermediate alloy and a Cu-rare earth intermediate alloy are prepared at first, and then the Cu-Zr intermediate alloy and the Cu-rare earth intermediate alloy are smelted and subjected to mould casting with copper, zinc, silver and titanium to form a cast ingot, the cast ingot is subjected to hot extrusion to obtain a bar billet, the bar billet is subjected to solution treatment, the treated alloy is subjected to drawing deformation, and then subjected to aging treatment to prepare the high-strength and high-conductivity rare earth copper alloy. The conductivity, elongation, strength and softening temperature of the alloy disclosed by the invention can be greatly improved; the machining performances of the alloy are remarkably improved; the manufacturability of the alloy can be changed, thus benefiting refining, degassing and microalloying; and the requirements of a material for the industrial field of contact lines on the performances of copper alloys can be met well. The alloy disclosed by the invention is simple in preparation process, short in process flow, high in strength, good in conductivity and excellent in hot-working property.
Owner:HENAN UNIV OF SCI & TECH

Production technique of xylose

The invention discloses a production technique of xylose. The production technique comprises the following steps: pulverizing, boiling with high-temperature water, hydrolyzing, decolorizing, refining, carrying out continuous film concentration, carrying out steam vaporization concentration, crystallizing, centrifuging and drying, thereby finally obtaining the crystalline xylose finished product. The xylose mother solution is sold as the byproduct and used as the raw material for preparing the caramel pigment product. The corn cobs are pulverized, thereby increasing the specific area, shortening the contact and soak time, enhancing the hydrolysis efficiency, and increasing the xylose yield. The hydrochloric acid is used for hydrolyzing the corn cobs to prepare the xylose, thereby saving the subsequent decolorant consumption, and reducing the environmental pollution. The continuous film concentration technique is adopted to partially substitute the steam vaporization technique, thereby having favorable energy-saving effect. The technique has the advantages of high waste acid/alkali recovery efficiency and favorable effect, and can save the acid/alkali consumption. The technique simplifies the technical process, shortens the production cycle, enhances the production efficiency, lowers the xylose production cost and reduces the wastewater emission.
Owner:HARBIN YOULI XYLITOL TECH CO LTD

Method for synchronously preparing walnut oil and walnut protein peptide by microwave-assisted protease hydrolysis

The invention provides a method for synchronously preparing walnut oil and walnut protein peptide by microwave-assisted protease hydrolysis, comprising the following steps of: grinding walnut raw materials into walnut powder, adding 100,000 to 1000,000 units of protease or composite protease to 1kg of walnut powder, adding water in the mass ratio of the walnut powder to the water is 1: (0.5-20), and then performing microwave processing for 1-10 minutes under the stirring condition of 60 to 300rpm when the microwave power is 10 to 1000 W / L and the temperature is 35 to 65 DEG C, and performing centrifugal separation of oil phase, aqueous phase and solid phase after the reaction ends, wherein the oil phase is walnut oil, the aqueous phase is walnut protein peptide, and the solid phase is residues. The method provided by the invention has mild extraction condition and excellent product performance, and can improve the efficiency of ingress of oil. Furthermore, the obtained walnut oil is higher in quality and is easy to refine; the processing time is greatly shortened by microwave-assisted extraction; the oil phase, the aqueous phase and the solid phase residues can be separated at the same time, therefore, the production efficiency is efficiently improved; and no waste water, waste air or waste residues exists in the producing process, therefore, the invention is environmentally-friendly.
Owner:KUNMING UNIV OF SCI & TECH

Process for preparing biodiesel by one-step method using biomass based sulfonation charcoal as fatty acid esterification and triglyceride transform esterification catalysts

The invention relates to a method for making biodiesel oil through adopting biomass-based sulfonated carbon as fatty acid esterifying and triglyceride transesterification catalyst one-step method. The method is as follows: biomass raw material containing abundant lignin is crushed and dipped in dilute sulfuric acid, and then is dried and carbonized at the low temperature to obtain biomass-based sulfonated carbon with a porous structure; and the biomass-based sulfonated carbon is taken as catalyst to make fatty acid mono-alkyl ester (biodiesel oil) through base oil fatty acid esterifying and triglyceride transesterification one-step method. The method solves the problems that: the manufacturing process of biodiesel oil through the prior acid-base catalysis method is limited by the acid value of base oil; and waste water discharge is great. The catalyst, which is insensitive to the by-product moisture generated during biodiesel oil production and is easy to separate, is propitious to the purification of crude glycerol; moreover, the catalyst, with low production cost, not only can be reused, but also can be abandoned to be used as a soil improvement material.
Owner:NANCHANG UNIV

Process method for microwave assistant supercritical extraction of active ingredients of curcuma

The invention discloses a process method for microwave assistant supercritical extraction of active ingredients of curcuma. In the method, the active ingredients, namely curcumin and fat soluble curcuma oil, of curcuma are extracted by the synergistic action of the microwave technology and the supercritical technology. The process method mainly comprises the following steps of: performing microwave intermittent sudden heating and then carbon dioxide (CO2) supercritical extraction; separating CO2 and curcuma oil in an analyzing kettle; and adding water or ethanol into curcuma residue in a solid-to-liquid weight ratio of 1:7-14, and performing microwave action, twice soaking, filtration, condensation and spray drying to obtain the curcumin. The process method solves the problem that in the prior art, only single active ingredient can be extracted or the compositions of the extract are not balanced, and realizes the extraction of two main active ingredients, namely curcuma oil and curcumin, of the curcuma at the same time, and the yield is over 8 percent and 13 percent respectively. The process method is the physical method and has the advantages of no product pollution, high purity, low cost, simple process and easy mass production.
Owner:GUANGZHOU RZN BIOTECH CO LTD
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