Three dimensional gradient metal hydroxide/oxide electrode material and manufacture method and application thereof
A technology of hydroxide and electrode materials, applied in electrode manufacturing, hybrid/electric double layer capacitor manufacturing, nanotechnology for materials and surface science, etc., can solve poor conductivity and ion dynamics, cycle performance and rate Poor performance, limited practical application, etc.
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[0196] Example 1
[0197] This embodiment provides a method for preparing a three-dimensional gradient metal hydroxide / oxide electrode material, which includes the following steps:
[0198] Follow Ni 2+ :Co 2+ The molar concentration ratio is 1:0, 2:1, 1:1, 1:2, 0:1, and 5 parts of nitrate solution with a total concentration of metal ions are 0.01mol / L; cut the foamed nickel into 1×1cm 2 Size, and after ultrasonic of 3mol / L hydrochloric acid solution for 10 minutes, remove the oxide film on the surface, and then wash it 3 times with deionized water and absolute ethanol; use the treated foamed nickel as the working electrode, saturated calomel and platinum As the reference electrode and the counter electrode, the three-electrode system was assembled, and the constant current 0.0005A was used on the CHI660E electrochemical workstation. 2+ :Co 2+ In the nitrate solution with molar ratio of 1:0, 2:1, 1:1, 1:2, 0:1, electrodeposit for 2 minutes respectively; use deionized water and anhy...
Example Embodiment
[0225] Example 2
[0226] This embodiment provides a method for preparing a three-dimensional gradient metal hydroxide / oxide electrode material, which includes the following steps:
[0227] Follow Ni 2+ :Co 2+ The molar concentration ratios are 4:1, 3:1, 2:1, and 1:1 respectively. 4 parts of sulfate solution with a total concentration of metal ions are 0.02mol / L; cut the foamed copper into a diameter of 1.8 cm round pole piece, and sonicated by 3mol / L hydrochloric acid solution for 10 minutes to remove the oxide film on the surface, and then washed with deionized water and absolute ethanol for 3 times; the treated foam copper is used as the working electrode, Saturated calomel and platinum tablets were used as the reference electrode and counter electrode, respectively, to assemble a three-electrode system. On the CHI660E electrochemical workstation, the constant current was 0.001A, and the Ni 2+ :Co 2+ In the nitrate solution with molar ratio of 4:1, 3:1,2:1, 1:1, electrodeposit f...
Example Embodiment
[0229] Example 3
[0230] This embodiment provides a method for preparing a three-dimensional gradient metal hydroxide / oxide electrode material, which includes the following steps:
[0231] Follow Ni 2+ :Co 2+ The molar ratios are 4:1, 3:1, 2:1, 1:1, and 4 parts of chloride salt solution with a total metal ion concentration of 0.02mol / L are configured; the copper foam is cut into a diameter of 1.8 cm round pole piece, and sonicated by 3mol / L hydrochloric acid solution for 10 minutes to remove the oxide film on the surface, and then washed with deionized water and absolute ethanol for 3 times; the treated foam copper is used as the working electrode, Saturated calomel and platinum tablets were used as the reference electrode and counter electrode, respectively, to assemble a three-electrode system. On the CHI660E electrochemical workstation, the constant current was 0.001A, and the Ni 2+ :Co 2+ In the nitrate solution with molar ratio of 4:1, 3:1,2:1, 1:1, electrodeposit for 2 minut...
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