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A kind of degumming agent of uv curing glue and its preparation method and degumming method

A degumming method and a degumming agent technology, which are applied in the processing of photosensitive materials, etc., can solve the problems of high degumming cost, consumption of concentrated sulfuric acid and hydrogen peroxide, etc., and achieve the effect of reducing degumming cost, reducing dosage, and simple preparation process

Active Publication Date: 2018-03-02
SUZHOU JIMCEL ELECTRONICS NEW MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The object of the present invention is to provide a kind of degumming agent for UV curable glue and its preparation method and degumming method for the technical problem that a large amount of concentrated sulfuric acid and hydrogen peroxide are consumed in the degumming process of UV curable adhesive bonded glass substrates, and the cost of degumming is high. , The preparation process of degumming agent for UV curable adhesive is simple and easy to operate, and at the same time greatly reduces the consumption of concentrated sulfuric acid and hydrogen peroxide, thereby reducing the degumming cost

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] 1. Preparation of UV curing adhesive debonding agent

[0033] Add 0.2 g of fatty alcohol polyoxyethylene ether into 97.8 g of pure water and stir to dissolve, then add 2.0 g of tetramethylammonium hydroxide and 100 g of methyl ethyl ketone into the prepared fatty alcohol polyoxyethylene ether aqueous solution, and stir evenly to obtain Debonding agent 1 for UV curing glue;

[0034] 2. Degumming method of UV curing glue

[0035] 1) In a constant temperature water bath at 60°C, soak 20 grams of the glass substrate in 80 grams of UV curable adhesive debonding agent 1, and soak for 1.5 hours, and the UV curable adhesive will be detached from the glass substrate;

[0036] 2) pour out the degumming agent of the UV curing glue of swelling;

[0037] 3) Add 20 grams of concentrated sulfuric acid solution to the peeled glass substrate, and soak in airtight at 60°C for 1.5 hours, and the trace amount of UV curable glue in the glass substrate is completely carbonized;

[0038] 4...

Embodiment 2

[0042] 1. Preparation of UV curing adhesive debonding agent

[0043] Add 1.0 gram of nonylphenol polyoxyethylene ether into 118 grams of pure water and stir to dissolve, then add 1.0 gram of tetraethylammonium hydroxide and 80 grams of N-methylpyrrolidone into the prepared nonylphenol polyoxyethylene ether aqueous solution, Stir evenly to obtain the debonding agent 2 of the UV curable adhesive;

[0044] 2. Degumming method of UV curing glue

[0045] 1) In a constant temperature water bath at 60°C, soak 20 grams of the glass substrate in the above-mentioned 100 grams of UV curing adhesive debonding agent 2, and soak in the air for 1.5 hours, and the UV curing adhesive will be detached from the glass substrate;

[0046] 2) Pour out the degumming agent of the swollen UV curing glue;

[0047] 3) Add 10 grams of concentrated sulfuric acid solution to the peeled glass substrate, and soak in airtight at 60°C for 1.5 hours, and the trace amount of UV curable glue in the glass substr...

Embodiment 3

[0052] 1. Preparation of UV curing adhesive debonding agent

[0053] Add 0.5 gram of fatty alcohol polyoxyethylene ether into 108 grams of pure water and stir to dissolve, then add 1.5 grams of tetrabutylammonium hydroxide and 90 grams of methyl isobutyl ketone into the prepared fatty alcohol polyoxyethylene ether aqueous solution, and stir evenly. Promptly obtain the debonding agent 3 of UV curing glue;

[0054] 2. Degumming method of UV curing glue

[0055] 1) In a constant temperature water bath at 60°C, soak 20 grams of the glass substrate in the above-mentioned 120 grams of UV curing adhesive debonding agent 3, and soak in the air for 1.5 hours, and the UV curing adhesive will be detached from the glass substrate;

[0056] 2) Pour out the degumming agent of the swollen UV curing glue;

[0057] 3) Add 10 grams of concentrated sulfuric acid solution to the peeled glass substrate, and soak in airtight at 60°C for 1.5 hours, and the trace amount of UV curable glue in the gl...

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Abstract

The invention relates to a degumming agent for UV curable glue, a preparation method and a degumming method thereof. The degumming agent of the UV curing adhesive contains 40%-50% of organic ketones, 0.5%-1.0% of organic quaternary ammonium base compounds, 0.1%-0.5% of surfactants, and the balance of pure water. Using the debonding agent of the present invention can take off most of the UV curing glue bonded in the glass substrate, and a small amount of UV curing glue adheres to the peeled glass substrate, and a small amount of concentrated sulfuric acid and hydrogen peroxide can be used to treat the UV curing glue. Perform a thorough degumming. Using the UV curing adhesive degumming agent of the present invention can reduce the consumption of concentrated sulfuric acid solution by 80% to 90%, reduce the consumption of hydrogen peroxide by 80% to 90%, and reduce the degumming cost. At the same time, the preparation process of the UV curing adhesive degumming agent of the present invention is simple, Easy to operate and can be recycled many times.

Description

technical field [0001] The invention relates to a degumming agent for UV curable adhesive, a preparation method and a degumming method thereof, in particular to a degumming agent for UV curable adhesive bonded glass substrates, a preparation method and a degumming method. Background technique [0002] As an economical, efficient, ecological, energy, and multifunctional adhesive, UV curing adhesive is widely used in many fields such as the manufacture of printed circuit boards, various plastic bonding, liquid crystal display installation, and electronic glass bonding. At present, concentrated sulfuric acid is mainly used as a debonding agent for UV curing adhesive bonding glass substrates. UV curing adhesive bonding glass substrates are soaked in hot concentrated sulfuric acid to completely carbonize the UV curing adhesive, and then add hydrogen peroxide solution to it. After carbonization, the concentrated sulfuric acid solution is decolorized and bleached, and the glass sub...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G03F7/42
Inventor 刘鸣孙宇亮于楼云刘利娟
Owner SUZHOU JIMCEL ELECTRONICS NEW MATERIAL
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