A kind of interface agent and preparation method thereof
A technology of interface agent and emulsifier, applied in the direction of filling slurry, etc., can solve the problems of paint peeling, time-consuming and laborious, and achieve the effect of preventing fading and discoloration, good waterproof performance, and strong alkali resistance.
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Embodiment 1
[0030] Pre-emulsion preparation: Add 62 parts of water, 3.5 parts of alkylphenol polyoxyethylene ether, 1.5 parts of styrene, 12.5 parts of isooctyl ester, and 17.5 parts of methacrylic acid into the emulsification tank, stir for 15- 20 minutes, obtain pre-emulsion A;
[0031] Polymerization reaction: Pour the bottom water into the reaction kettle, wait until the temperature in the kettle rises to 80-82°C, first add 0.25 parts of ammonium persulfate, and then drop in pre-emulsion A and 0.25 parts of ammonium persulfate at the same time , and control exactly 3 hours dripping, the total reaction time of the polymerization reaction is 3 hours;
[0032] Insulation: After the dropwise addition is completed, keep the temperature for 1 hour;
[0033] Adjust PH value and film formation: After heat preservation, add 1.5 parts of PH regulator to adjust the pH value of the product between 7-8, and finally add 1 part of film-forming aid, stir for 10 minutes, and obtain the described prod...
Embodiment 2
[0035] Pre-emulsion preparation: Add 60 parts of water, 4 parts of alkylphenol polyoxyethylene ether, 1 part of styrene, 13.5 parts of isooctyl ester, and 18 parts of methacrylic acid into the emulsification tank, stir for 15- 20 minutes, obtain pre-emulsion A;
[0036] Polymerization reaction: Pour the bottom water into the reaction kettle, wait until the temperature in the kettle rises to 80-82°C, first add 0.25 parts of ammonium persulfate, then drop in pre-emulsion A and 0.75 parts of ammonium persulfate at the same time , and control exactly 3 hours dripping, the total reaction time of the polymerization reaction is 3 hours;
[0037] Insulation: After the dropwise addition is completed, keep the temperature for 1 hour;
[0038] Adjust PH value and film formation: After heat preservation, add 2 parts of PH regulator to adjust the pH value of the product between 7-8, and finally add 0.5 parts of film-forming aid, stir for 10 minutes, and obtain the described product after ...
Embodiment 3
[0040] Pre-emulsion preparation: Add 64 parts of water, 3 parts of alkylphenol polyoxyethylene ether, 2 parts of styrene, 12 parts of isooctyl ester, and 16 parts of methacrylic acid into the emulsification tank, stir for 15- 20 minutes, obtain pre-emulsion A;
[0041] Polymerization reaction: Pour the bottom water into the reaction kettle, wait until the temperature in the kettle rises to 80-82°C, first add 0.25 parts of ammonium persulfate, then drop in pre-emulsion A and 0.75 parts of ammonium persulfate at the same time , and control exactly 3 hours dripping, the total reaction time of the polymerization reaction is 3 hours;
[0042] Insulation: After the dropwise addition is completed, keep the temperature for 1 hour;
[0043] Adjust PH value and film formation: After the heat preservation is over, add 1 part of PH regulator to adjust the pH value of the product between 7-8, and finally add 1 part of film-forming aid, stir for 10 minutes, and obtain the described product...
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