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Half-thermal-state thermal shock resistance experimental device and method for refractory material

A technology of refractory materials and experimental equipment, applied in the field of refractory materials, can solve the problem of inability to accurately simulate the working conditions of refractory materials in the chute area of ​​CDQ furnaces, and the inability to accurately evaluate the thermal shock resistance of refractory materials used in the chute area of ​​CDQ furnaces, etc. problem, to achieve the effect of solving the thermal shock resistance of the heating state

Active Publication Date: 2015-03-04
SHOUGANG CORPORATION +1
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The embodiment of the present application solves the problem that the thermal shock resistance test in the prior art cannot accurately simulate the working conditions of the refractory material in the chute area of ​​the CDQ furnace by providing a semi-hot state thermal shock resistance experimental device and method of the refractory material. Accurately evaluate the thermal shock resistance of the refractory materials used in the CDQ furnace chute area, realize the accurate simulation of the working conditions of the CDQ furnace chute area refractory materials, and accurately restore the refractory materials used in the CDQ furnace chute area after several times of rapid cooling. The loss of flexural strength after heating and quantifying the semi-hot thermal shock resistance of refractory materials

Method used

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  • Half-thermal-state thermal shock resistance experimental device and method for refractory material

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Experimental program
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Effect test

Embodiment 1

[0069] S1: Cut 9 pieces of flexural specimens with a size of 40×40×160mm from corbel bricks in the chute area of ​​the CDQ furnace, of which 3 pieces are the first experimental sample group and 3 pieces are the second experimental sample group Sample group, 3 pieces are the third experimental sample group.

[0070] S2: Place the first experimental sample group in the flexural tester, and test at room temperature to obtain the average value P of the first room temperature flexural strength of the 3 flexural samples c = 10 MPa.

[0071] S3: Place the second experimental sample group in the flexural tester, and test in a high temperature environment to obtain the average value P of the high temperature flexural strength of the 3 flexural samples g =10.6Mpa, where the high temperature is controlled at 1000°C.

[0072] S4: The third experimental sample group is placed in a thermal shock furnace for heating, the heating temperature is controlled at 300° C., and the heating time is...

Embodiment 2

[0079] S1: Cut 9 pieces of flexural specimens with a size of 40×40×160mm from corbel bricks in the chute area of ​​the CDQ furnace, of which 3 pieces are the first experimental sample group and 3 pieces are the second experimental sample group Sample group, 3 pieces are the third experimental sample group.

[0080] S2: Place the first experimental sample group in the flexural tester, and test at room temperature to obtain the average value P of the first room temperature flexural strength of the 3 flexural samples c = 10 MPa.

[0081] S3: Place the second experimental sample group in the flexural tester, and test in a high temperature environment to obtain the average value P of the high temperature flexural strength of the 3 flexural samples g =10.6Mpa, where the high temperature is controlled at 1000°C.

[0082] S4: The third experimental sample group is placed in a thermal shock furnace for heating, the heating temperature is controlled at 500° C., and the heating time is...

Embodiment 3

[0089] S1: Cut 9 pieces of flexural specimens with a size of 40×40×160mm from corbel bricks in the chute area of ​​the CDQ furnace, of which 3 pieces are the first experimental sample group and 3 pieces are the second experimental sample group Sample group, 3 pieces are the third experimental sample group.

[0090] S2: Place the first experimental sample group in the flexural tester, and test at room temperature to obtain the average value P of the first room temperature flexural strength of the 3 flexural samples c = 10 MPa.

[0091] S3: Place the second experimental sample group in the flexural tester, and test in a high temperature environment to obtain the average value P of the high temperature flexural strength of the 3 flexural samples g =10.6Mpa, where the high temperature is controlled at 1000°C.

[0092] S4: The third experimental sample group is placed in a thermal shock furnace for heating, the heating temperature is controlled at 700° C., and the heating time is...

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Abstract

The invention relates to a half-thermal-state thermal shock resistance experimental device and a half-thermal-state thermal shock resistance experimental method. The device comprises a fracture resistance experiment instrument, a thermal shock furnace, a fan and a temperature measurer, wherein the fracture resistance experiment instrument is used for determining normal-temperature breaking strength and high temperature breaking strength of an experimental test sample; the thermal shock furnace is used for heating the experimental test sample; the fan is used for cooling the heated experimental test sample; the temperature measurer is used for detecting the surface temperature of the cooled experimental test sample. The method comprises the steps of preparing the experimental test sample; acquiring first normal temperature breaking strength Pc; acquiring high temperature breaking strength Pg; heating and cooling the experimental test sample; stopping cooling the experimental test sample when the surface temperature of the experimental test sample is detected by the temperature measurer to reach a set value; sequentially and alternately carrying out the heating process and the cooling process to set times; acquiring second normal temperature breaking strength Pr; calculating a strength loss rate by virtue of a strength loss formula. By adopting the experimental device and method, the application working condition of the refractory material in a chute area of a dry quenching furnace can be accurately simulated, and the half-thermal-state thermal shock resistance of the refractory material can be quantized.

Description

technical field [0001] The invention relates to the technical field of refractory materials, in particular to a semi-hot state thermal shock resistance experimental device of refractory materials and a method thereof. Background technique [0002] The main equipment of CDQ is the masonry of the CDQ furnace, which belongs to the vertical kiln structure. It is a cylindrical upright masonry in a positive pressure state. The entire CDQ furnace is surrounded by an iron shell, and the inner layer is made of different refractory bricks. From top to bottom, the furnace body can be divided into pre-storage room, chute area and cooling room. The refractory material (commonly known as corbel brick) in the chute area is not only impacted by the coke flowing downward, but also scoured by the coke powder entrained by the upward circulating gas. Moreover, the temperature of coke, circulating gas and refractory material changes continuously along the height of the chute, especially when th...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N3/60
Inventor 钟凯张效鹏朱长军崔园园曹勇祝少军薛立民彭军山杨庆彬马泽军
Owner SHOUGANG CORPORATION