Technique and equipment for preparing high-temperature super-conduction strip materials by virtue of laser chemical vapor deposition method

A technology of chemical vapor deposition and high-temperature superconducting strips, which is applied in the usage of superconducting elements, gaseous chemical plating, superconducting devices, etc., can solve the problems of slow deposition speed, reduction of activation energy of reaction between raw material molecules, and low production efficiency And other issues

Inactive Publication Date: 2015-03-18
WUHAN XINGUI TECH QIANJIANG CO LTD
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Problems solved by technology

[0005] The purpose of the present invention is to provide a technology and equipment for high-speed and continuous preparation of second-generation high-temperature superconducting strips using liquid spray atomization-multiple eutectoid laser chemical vapor deposition, so as to solve the problem of large-scale preparation of conventional chemical vapor deposition. Difficulties Existing in the Second Generation High Temperature Superconducting Tape Products
[0006] Aiming at the problems of slow deposition rate and low production efficiency of the conventional chemical vapor deposition method, the solution of the patent of the present invention is: by introducing the laser into the reaction chamber to irradiate the surface of the substrate, the reaction activation energy between the raw material molecules is greatly reduced , so the second-generation high-temperature superconductor and its buffer layer film can be prepared at a very high rate

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  • Technique and equipment for preparing high-temperature super-conduction strip materials by virtue of laser chemical vapor deposition method

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Embodiment approach

[0013] When the equipment is running, the main reaction chamber 10, the two secondary reaction chambers 14 and the chamber connecting pipe 15 will reduce the pressure of the chamber to the required value under the action of the vacuum pump 13, providing necessary conditions for the preparation of the film.

[0014] The liquid raw material in the liquid raw material tank 1 is drawn by the liquid raw material supply part 3 through the liquid raw material extraction pipe 2, and is continuously and stably sent to the pressure chamber 5 via the liquid raw material delivery pipe 4. The gas in the carrier gas storage tank 6 generates pressure in the pressure chamber 5 and quickly presses out the liquid raw material that has been pressured into the pressure chamber 5, and the liquid raw material is thus atomized into small droplets. When the atomized small droplets are sprayed to the wall of the spray atomization-multi-eutectoid volatilization cavity 7, the solvent in the small droplets v...

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Abstract

The invention relates to a technique and equipment for rapidly and continuously preparing second-generation high-temperature super-conduction strip materials by virtue of a liquid injection atomization-multielement eutectoid laser chemical vapor deposition method. According to a liquid raw material supply system of the equipment, the problems that accurate, stable and continuous raw material steam cannot be supplied for a long time by virtue of a traditional chemical vapor deposition method, and components of a thin film cannot be accurately controlled in a preparation process of a multielement thin film are solved. Based on the liquid raw material supply system of the equipment, by illuminating the surface of a substrate by virtue of laser, the reaction activation energy among molecules of a gas phase raw material is substantially reduced, and the speed of the chemical reaction is increased. By virtue of a compound roller transmission system of the equipment, long flexible substrate strip materials can be gradually transported to a deposition region of a heating table, so as to rapidly and continuously prepare second-generation high-temperature super-conduction strip material products.

Description

1. Technical Field: [0001] The present invention is a technology and equipment for high-speed and continuous preparation of second-generation high-temperature superconducting tapes by using a liquid spray atomization-multiple eutectoid laser chemical vapor deposition method, and relates to a second-generation high-temperature superconducting film with high electrical properties and The high-speed and continuous preparation technology of the buffer layer film belongs to the technical field of superconducting materials. 2. Background technology: [0002] A material whose resistance is completely zero at low temperatures is called a superconducting material, and it is considered one of the greatest discoveries of the 20th century. Superconducting technology is an important direction of high-tech development in this century. It has important practical significance and huge development prospects in high-tech fields such as energy, transportation, industry, medical treatment, biology,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C16/54C23C16/448C23C16/455C23C16/48C23C16/40H01B12/00
CPCC23C16/40C23C16/448C23C16/455C23C16/483C23C16/54H01B12/00Y02E40/60
Inventor 赵培徐源来
Owner WUHAN XINGUI TECH QIANJIANG CO LTD
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