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Technology and equipment for preparing high-temperature superconducting strips by laser chemical vapor deposition

A chemical vapor deposition, high temperature superconducting tape technology, applied in the use of superconductor elements, gaseous chemical plating, superconducting devices, etc., can solve the problem of slow deposition speed, reduce the activation energy of intermolecular reaction of raw materials, and low production efficiency And other issues

Inactive Publication Date: 2018-02-16
WUHAN XINGUI TECH QIANJIANG CO LTD
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Problems solved by technology

[0005] The purpose of the present invention is to provide a technology and equipment for high-speed and continuous preparation of second-generation high-temperature superconducting strips using liquid spray atomization-multiple eutectoid laser chemical vapor deposition, so as to solve the problem of large-scale preparation of conventional chemical vapor deposition. Difficulties Existing in the Second Generation High Temperature Superconducting Tape Products
[0006] Aiming at the problems of slow deposition rate and low production efficiency of the conventional chemical vapor deposition method, the solution of the patent of the present invention is: by introducing the laser into the reaction chamber to irradiate the surface of the substrate, the reaction activation energy between the raw material molecules is greatly reduced , so the second-generation high-temperature superconductor and its buffer layer film can be prepared at a very high rate

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  • Technology and equipment for preparing high-temperature superconducting strips by laser chemical vapor deposition

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Embodiment approach

[0013] The device for preparing high-temperature superconducting tape by laser chemical vapor deposition method provided in this embodiment includes: liquid raw material box 1, liquid raw material extraction pipe 2, liquid raw material supply part 3, liquid raw material delivery pipe 4, pressure chamber 5, carrier gas Storage tank 6, liquid spray atomization-multivariate eutectoid volatilization chamber 7, raw material vapor delivery pipe 8, double-layer raw material mixing nozzle 9, main reaction chamber 10, reactant gas storage tank 11, laser introduction window 12, vacuum pump 13 , secondary reaction chamber 14, chamber connecting pipe 15, spiral strip winding roller 16, heating table 17, strip winding disk 18, strip conveying disk 19, long flexible substrate strip 20, strip line speed measuring wheel 21 , continuous laser generator 22, laser beam amplifier 23, equipment control cabinet 24 and connecting cable 25, the secondary reaction chamber 14, the chamber Unicom pipe 15...

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Abstract

The invention relates to a technique and equipment for rapidly and continuously preparing second-generation high-temperature super-conduction strip materials by virtue of a liquid injection atomization-multielement eutectoid laser chemical vapor deposition method. According to a liquid raw material supply system of the equipment, the problems that accurate, stable and continuous raw material steam cannot be supplied for a long time by virtue of a traditional chemical vapor deposition method, and components of a thin film cannot be accurately controlled in a preparation process of a multielement thin film are solved. Based on the liquid raw material supply system of the equipment, by illuminating the surface of a substrate by virtue of laser, the reaction activation energy among molecules of a gas phase raw material is substantially reduced, and the speed of the chemical reaction is increased. By virtue of a compound roller transmission system of the equipment, long flexible substrate strip materials can be gradually transported to a deposition region of a heating table, so as to rapidly and continuously prepare second-generation high-temperature super-conduction strip material products.

Description

1. Technical field: [0001] The invention is a technology and equipment for high-speed and continuous preparation of second-generation high-temperature superconducting strips using liquid spray atomization-multivariate eutectoid laser chemical vapor deposition, and relates to second-generation high-temperature superconducting thin films with high electrical properties and The high-speed and continuous preparation technology of the buffer layer thin film belongs to the technical field of superconducting materials. 2. Background technology: [0002] Materials whose electrical resistance is completely zero at low temperatures are called superconducting materials, and it is considered one of the greatest discoveries of the 20th century. Superconducting technology is an important direction of high-tech development in this century. It has important practical significance and great development prospects in high-tech fields such as energy, transportation, industry, medical treatment...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C16/54C23C16/448C23C16/455C23C16/48C23C16/40H01B12/00
CPCC23C16/40C23C16/448C23C16/455C23C16/483C23C16/54H01B12/00Y02E40/60
Inventor 赵培徐源来
Owner WUHAN XINGUI TECH QIANJIANG CO LTD
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