Method for treating backflow fracturing fluid reclaimed from exploitation of shale gas
A fracturing flowback fluid and treatment method technology, applied in mining wastewater treatment, water/sewage treatment, water treatment parameter control, etc.
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Embodiment 1
[0036] As a preferred embodiment of the present invention, the steps of the present invention are as follows:
[0037] S1. First detect the ion content in the flowback liquid, and the control ranges of the ion content in the flowback liquid are: K + ≤1500 mg / L 、Ca 2+ ≤600 mg / L, Na + ≤2000 mg / L, Mg 2+ ≤1000 mg / L, NH 4 + ≤600 mg / L, total Fe≤25 mg / L, Cl - ≤3000 mg / L 、Al 3+ ≤30 mg / L, SO 4 2- ≤200 mg / L, COD≤300 mg / L, it is regarded as reaching the standard, and the flowback liquid that meets the standard is put into the container for standby;
[0038] S2. Before injecting the spare up-to-standard flowback fluid into the ground for fracturing, use the following two formulas for comparative testing:
[0039] (1) The newly configured clear water slick water for comparison: 99.9 parts of clear water or tap water + 0.1 part of drag reducing agent;
[0040] (2) The spare flowback liquid slippery water in the container: 99.9 parts of flowback liquid + 0.1 part of drag reducer; ...
Embodiment 2
[0044] As the best implementation mode of the present invention, this scheme carries out the following treatment to the flowback liquid with unqualified performance in step S2 of embodiment 1 and the flowback liquid with ion content not up to standard in step S1:
[0045] S3. After the flowback liquid tested by S1, if the ion content is not up to the standard, or the flowback liquid with unqualified performance after the step S2 is filtered by nanotechnology to remove excess ions in the flowback liquid, the flowback liquid After treatment, metal ions should be controlled within the range controlled by step S1;
[0046] S4. Re-sampling and testing the flowback liquid after filtration, using atomic absorption spectrometry for component detection, and the flowback liquid component detection items include: K + , Ca 2+ 、Na + , Mg 2+ , total Fe, Sr 2+ 、Al 3+ NH 4 + , Cl - , SO 4 2- , SRB, COD; when the performance reaches K + ≤1500 mg / L 、Ca 2+ ≤600 mg / L, Na + ≤2000 mg...
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