Method for preparing tobacco herbal fragrant substance for cigarette solution of electronic cigarette

A technology of e-cigarette liquid and fragrance substances, which is applied in the fields of tobacco, tobacco processing, application, etc., can solve the problems of low extraction rate of solid materials, high extraction pressure, and low mass transfer efficiency, so as to ensure product quality stability and Safety, enhanced extraction process, high yield effect

Active Publication Date: 2015-03-25
CHINA TOBACCO SHANDONG IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the current supercritical fluid extraction still has problems such as high extraction pressure, long extraction time, low mass transfer efficiency, and low extraction rate of solid materials, and there is no suitable method for preparing tobacco aroma substances for electronic cigarette liquids.

Method used

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  • Method for preparing tobacco herbal fragrant substance for cigarette solution of electronic cigarette
  • Method for preparing tobacco herbal fragrant substance for cigarette solution of electronic cigarette
  • Method for preparing tobacco herbal fragrant substance for cigarette solution of electronic cigarette

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] The waste tobacco leaves are cleaned of impurities, dried to a moisture content of 6%, and pulverized into 20 meshes. Weigh 1 kg of pulverized waste tobacco leaves, add 2 kg of ethanol with a mass fraction of 95% and soak for 24 hours, use an ultrasonic cell pulverizer to perform ultrasonic cell pulverization treatment for 15 min, and then put it into a 5 L high-voltage pulse electric field-strengthened supercritical CO 2 Extraction kettle for extraction. Wherein: ultrasonic condition is: ultrasonic frequency 20KHz, ultrasonic power 400W, ultrasonic interval 15s, extraction condition is: electric field strength 20KV / cm, pulse number is 10, extraction pressure 25MPa, extraction temperature 50 ℃, extraction time 2h, CO 2 The flow rate is 15L / h, and the amount of entrainer (propylene glycol / 95% ethanol / distilled water=4 / 3 / 3 (mass ratio)) is CO 2 4% of the volume. Pass the extracted mixture into separation kettle 1 and separation kettle 2 for separation, and recover CO 2...

Embodiment 2

[0023] The waste tobacco leaves are cleaned of impurities, dried to a moisture content of 6%, and pulverized into 30 meshes. Weigh 1 kg of pulverized waste tobacco leaves, add 2.5 kg of ethanol with a mass fraction of 98% and soak for 26 h, use an ultrasonic cell pulverizer to perform ultrasonic cell pulverization for 20 min, and then put it into 5 L of supercritical CO 2 Extraction kettle for extraction. Wherein: ultrasonic condition is: ultrasonic frequency 20KHz, ultrasonic power 400W, ultrasonic interval 10s, extraction condition is: electric field intensity 40KV / cm, pulse number is 12, extraction pressure 25MPa, extraction temperature 55 ℃, extraction time 2h, CO 2 The flow rate is 20L / h, and the amount of entrainer (propylene glycol / 95% ethanol / distilled water=4 / 3 / 3 (mass ratio)) is CO 2 8% of the volume. Pass the extracted mixture into separation kettle 1 and separation kettle 2 for separation, and recover CO 2 . The separation conditions are as follows: the pressur...

Embodiment 3

[0026]The waste tobacco leaves are cleaned of impurities, dried to a moisture content of 6%, and pulverized into 20 meshes. Weigh 1 kg of pulverized waste tobacco leaves, add 1.5 kg of ethanol with a mass fraction of 90% and soak for 20 h, use an ultrasonic cell pulverizer to perform ultrasonic cell pulverization for 15 min, and then put it into a supercritical high-voltage pulsed electric field-strengthened supercritical cell with a volume of 5 L. CO 2 Extraction kettle for extraction. Wherein: ultrasonic condition is: ultrasonic frequency 20KHz, ultrasonic power 400W, ultrasonic interval 10s, extraction condition is: electric field strength 20KV / cm, pulse number is 8, extraction pressure 25MPa, extraction temperature 40 ℃, extraction time 1.5h, CO 2 The flow rate is 10L / h, and the amount of entrainer (propylene glycol / 95% ethanol / distilled water=4 / 3 / 3 (mass ratio)) is CO 2 4% of the volume. Pass the extracted mixture into separation kettle 1 and separation kettle 2 for se...

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Abstract

The invention discloses a method for preparing a tobacco herbal fragrant substance for cigarette solution of an electronic cigarette. The method comprises the steps that waste and inferior tobaccos are extracted in an ultrasound-enhanced supercritical extraction device for 1.5-2 hours at the temperature of 40-55 DEG C in the presence of an entrainer under the conditions that the ultrasonic frequency is 20KHz, the ultrasonic power is 100W, the flow rate of carbon dioxide of 10-20L / h and the extraction pressure is 15-25 MPa, so as to prepare a mixed solution of carbon dioxide and the tobacco herbal fragrant substance, wherein the entrainer is a mixed solvent of propylene glycol, ethanol and distilled water; the mixed solution is separated by virtue of a separation kettle at temperature of 45- 60 DEG C under the separation pressure of 7-12MPa to obtain the tobacco herbal fragrant substance. The tobacco herbal fragrant substance contains tobacco natural fragrant substance components, nicotine and the like and is applied to the cigarette solution of the electronic cigarette so that the cigarette solution of the electronic cigarette is endowed with the same sense organ characteristic and a satisfaction sense of smoking as common cigarettes. The extraction method is easy to carry out, low in cost, and stable and safe in product quality; the environment pollution is avoided; compared with the conventional supercritical extraction process, the method has the advantage that material consumption and energy consumption are reduced.

Description

technical field [0001] The invention relates to a preparation method of a tobacco aroma substance used in electronic cigarette liquid. Background technique [0002] Electronic cigarettes, also known as electronic cigarettes, are mainly used to quit smoking and replace cigarettes. It has the same appearance and taste similar to cigarettes, and even has a lot more flavor than ordinary cigarettes. It can also suck out smoke, taste and feeling like cigarettes. E-cigarettes do not have other harmful components such as tar and suspended particles in cigarettes, and there is no diffuse or lingering second-hand smoke in e-cigarettes. E-cigarette liquid is the essence extracted from plants and added with edible flavors. It has strong oxidation resistance and does not contain harmful substances such as carbon monoxide and tar. In order to ensure that e-cigarettes can bring smokers the same sensory quality as cigarettes, it is necessary to add spices, nicotine and other substances t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24B15/16
CPCA24B15/16C11B9/022C11B9/025
Inventor 刘新建朱友民王钧郑宏伟周仕禄董全江史先鑫
Owner CHINA TOBACCO SHANDONG IND
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