Urea-formaldehyde glue and preparation method thereof
A technology of glue and urine glue, applied in the direction of adhesives, adhesive types, aldehyde/ketone condensation polymer adhesives, etc., to achieve good impregnation effect and high hardness
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Embodiment 1
[0018] A urea glue, which is composed of the following substances in parts by weight: 4200kg of formaldehyde, 2400kg of urea, 300kg of saffron extract, and 1000kg of water.
[0019] The extraction method of the saffron extract is as follows: dry 1500kg of the sage, crush it, add 3000L of ethanol to dissolve, heat to 40-60 degrees and stir for 1-5h, take the solution, evaporate to dryness and reflux the ethanol to obtain the sage extract.
[0020] The preparation method of above-mentioned urine glue glue is carried out according to the following steps:
[0021] (1) Take 4200kg of formaldehyde, add 1000kg of water, and use sodium hydroxide solution to adjust the pH to 8.0;
[0022] (2) Add 1400kg of urea and 300kg of saffron extract, and turn off the steam when the temperature rises to 65 degrees;
[0023] (3) Heat up to 90 degrees, keep it warm for 20 minutes, use formic acid to adjust the pH to 4.2, react for 20 minutes, and measure the water solubility ratio to 1:2.5;
[00...
Embodiment 2
[0028] A urea glue, which is composed of the following substances in parts by weight: 3500kg of formaldehyde, 2500kg of urea, 200kg of sage extract and 900kg of water.
[0029] The extraction method of the saffron extract is as follows: dry 1200kg of the sage, crush it, add 2400L of ethanol to dissolve, heat to 40-60 degrees and stir for 1-5h, take the solution, evaporate to dryness and reflux the ethanol to obtain the sage extract.
[0030] The preparation method of above-mentioned urine glue glue is carried out according to the following steps:
[0031] (1) Take 3500kg of formaldehyde, add 900kg of water, and use sodium hydroxide solution to adjust the pH to 8.2;
[0032] (2) Add 1500kg of urea, 200kg of saffron extract, and turn off the steam when the temperature rises to 65 degrees;
[0033] (3) Heat up to 92 degrees, keep warm for 25 minutes, use formic acid to adjust the pH to 4.3, react for 20 minutes, and measure the water solubility ratio to be 1:3;
[0034] (4) Use...
Embodiment 3
[0038] A urea glue, which is composed of the following substances in parts by weight: 5000kg of formaldehyde, 3000kg of urea, 500kg of saffron extract, and 1200kg of water.
[0039] The extraction method of the saffron extract is as follows: dry 2500kg of the sage, crush it, add 5000L of ethanol to dissolve, heat to 40-60 degrees and stir for 1-5h, take the solution, evaporate to dryness and reflux the ethanol to obtain the sage extract.
[0040] The preparation method of above-mentioned urine glue glue is carried out according to the following steps:
[0041] (1) Take 5000kg of formaldehyde, add 1200kg of water, and use sodium hydroxide solution to adjust the pH to 8.5;
[0042] (2) Add 2000kg of urea and 500kg of saffron extract, and turn off the steam when the temperature rises to 65 degrees;
[0043] (3) Heat up to 95 degrees, keep warm for 30 minutes, use formic acid to adjust the pH to 4.4, react for 25 minutes, and measure the water solubility ratio to 1:3.5;
[0044]...
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