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A method for cleaning membrane organic solvent pollutants

A technology of organic solvents and pollutants, applied in the field of membrane cleaning, can solve the problems of reducing the service life of nanofiltration membranes, membrane damage, membrane pollution, etc., and achieve the effect of short cleaning time and good cleaning effect

Active Publication Date: 2017-05-17
ZHEJIANG UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Its disadvantage is that organic solvents will cause membrane pollution as a pollutant. If they are not cleaned, they will cause irreversible membrane damage and reduce the service life of nanofiltration membranes.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] After the mixture of rice bran oil and acetone is separated by the membrane, the nanofiltration membrane is cleaned:

[0024] (1) Cleaning of solute pollutant rice bran oil: first clean with the same organic solvent acetone as the organic solvent used in the application of membrane production, the cleaning process is: first empty the mixture of rice bran oil and acetone in the nanofiltration membrane device , add the same organic solvent acetone as the organic solvent used in the application of film production, at 0.3kg / cm 2 Under the pulse frequency of / min, the membrane pressure of the nanofiltration membrane device rises from low pressure to high pressure. 2 The pulse frequency of / min drops from the high pressure state to the low pressure state, and maintains in the low pressure state for 2 minutes, and takes this as a cycle, and circulates for 20 minutes; the low pressure state is 2kg / cm 2 , the high pressure state is 18kg / cm 2 ;

[0025] (2) Cleaning of organic...

Embodiment 2

[0031] After the mixture of soybean oil and n-hexane is separated by membrane, the nanofiltration membrane is cleaned:

[0032] (1) Cleaning of solute pollutant soybean oil: first clean with the same organic solvent n-hexane as the organic solvent used in the production of the applied membrane, the cleaning process is: first empty the soybean oil and normal hexane in the nanofiltration membrane device The mixture, adding the same organic solvent n-hexane as the organic solvent used in film production, at 0.2kg / cm 2 Under the pulse frequency of / min, the membrane pressure of the nanofiltration membrane device rises from low pressure to high pressure. 2The pulse frequency of / min drops from the high pressure state to the low pressure state, and maintains in the low pressure state for 2 minutes, and takes this as a cycle, and circulates for 20 minutes; the low pressure state is 2kg / cm 2 , the high pressure state is 18kg / cm 2 ;

[0033] (2) Cleaning of organic solvent pollutant...

Embodiment 3

[0039] After the mixture of tuna oil and n-heptane is separated by membrane, the nanofiltration membrane is cleaned:

[0040] (1) Cleaning of solute pollutant tuna oil: first clean with the same organic solvent n-heptane as the organic solvent used in the production of the applied membrane, and the cleaning process is: first empty the tuna oil and n-heptane in the nanofiltration membrane device Mixture of alkanes, add the same organic solvent as the organic solvent used in the production of the film, at 0.3kg / cm 2 Under the pulse frequency of / min, the membrane pressure of the nanofiltration membrane device rises from low pressure to high pressure. 2 The pulse frequency of / min drops from the high pressure state to the low pressure state, and maintains in the low pressure state for 2 minutes, and takes this as a cycle, and circulates for 20 minutes; the low pressure state is 2kg / cm 2 , the high pressure state is 16kg / cm 2 ;

[0041] (2) Cleaning of organic solvent pollutant...

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PUM

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Abstract

The invention discloses a method for cleaning organic solvent pollutants of a membrane. The method comprises the four steps of cleaning solute pollutants; cleaning organic solvent pollutants; removing an organic solvent cleaning agent; and removing alkaline substance aqueous solution. The method has the advantages of good cleaning effect and short cleaning time.

Description

[0001] (1) Technical field [0002] The invention relates to a membrane cleaning method, in particular to a membrane cleaning method capable of effectively cleaning organic solvent pollutants. The method of the invention is suitable for cleaning aromatic polyamide composite roll membranes and belongs to the technical field of membrane cleaning. [0003] (2) Background technology [0004] Membrane separation is a new separation technology that appeared in the early 20th century and rose rapidly after the 1960s. Membrane separation technology is a method of separation using a semi-permeable membrane, which is driven by the pressure difference or potential difference on both sides of the membrane at room temperature to separate and purify the solute. Membrane separation technology has the functions of separation, concentration, purification and refining, and has the advantages of high efficiency, energy saving, environmental protection, molecular-level filtration, simple filtratio...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D65/02B01D65/06
Inventor 方亦舟丁玉庭刘建华
Owner ZHEJIANG UNIV OF TECH