Preparation method of compounded fruit and vegetable cleaning agent of kadsura longepedunculata extract and oil-tea-cake extract

A fruit and vegetable cleaning agent, the technology of Schisandra chinensis, applied in the direction of chemical instruments and methods, surface active non-soap compounds and washing compositions, detergent compositions, etc., can solve the problem of insufficient antibacterial properties of effective antibacterial components in extraction process optimization, Insufficient antibacterial effect of antibacterial agents, loss of antibacterial active ingredients and other problems, to achieve the effect of sterilization and broad antibacterial spectrum, good bactericidal effect, and complementary bactericidal spectrum

Inactive Publication Date: 2015-07-01
ZHONGKAI UNIV OF AGRI & ENG +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are still many problems in the industrial application of its antibacterial active ingredients
For example: the antibacterial effect of the antibacterial active ingredients is affected by the pH value of the solvent; the ordinary extraction process will cause a large loss of antibacterial active ingredients in Schisandra chinensis and camellia oleifera cake, the antibacterial effect is not ideal, and the end product contains more impurities, etc. Difficult problem; with the same dosage, the antibacterial effect of the antibacterial agent extracted from Schisandra chinensis and Camellia oleifera cake is not as good as that of...

Method used

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Examples

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preparation example Construction

[0031] A preparation method of a fruit and vegetable cleaning agent compounded by Schisandra chinensis extract and Camellia oleifera cake extract, comprising the following steps:

[0032] 1) Extraction: Extract the southern Schisandra powder with a mixture of ethanol and acetone with a volume ratio of (50~55): 100 as the extractant, filter the extract, take the filtrate, and then concentrate the filtrate to obtain the flavonoid concentration 0.8~1.0mg / mL crude extract solution of Schisandra chinensis;

[0033] Extract the camellia oleifera cake powder with an ethanol solution with a volume concentration of 60-65% as an extractant, filter the extract, take the filtrate, and then concentrate the filtrate to obtain a crude oil-tea oleifera cake with a saponin concentration of 1.6-2.1 mg / mL. extract solution;

[0034] 2) Purification: firstly pretreat the resin, put the resin into a column, and adjust the pH value of the crude extract solution of Schisandra chinensis and the crud...

Embodiment 1

[0046] Example 1 A preparation method of a fruit and vegetable cleaning agent compounded with Schisandra chinensis extract and camellia oleifera cake extract

[0047] 1) Pretreatment: Wash and drain the fresh fruit of Schisandra chinensis, air-dry at 60-70°C until the water content is below 8%, pulverize, and pass through a 20-mesh sieve to obtain Schisandra chinensis powder, which is sealed and stored for later use;

[0048] Pulverize the camellia oleifera cake and pass through a 20-mesh sieve to obtain the camellia oleifera cake powder, which is sealed and stored for later use;

[0049] 2) Extraction: Place the Schisandra chinensis powder obtained in the previous step in a condensation reflux device (this device is convenient for the recovery of the extractant in the subsequent vacuum distillation process), and add ethanol and acetone with a volume ratio of (50~55):100 The mixed solution is used as the extractant, the ratio of solid to liquid is 1g: (40~50) mL, after leach...

Embodiment 2

[0054] Example 2 A preparation method of a fruit and vegetable cleaning agent compounded with Schisandra chinensis extract and camellia oleifera cake extract

[0055] 1) Pretreatment: Wash and drain the fresh fruit of Schisandra chinensis, air-dry at 65°C until the water content is below 8%, pulverize, pass through a 20-mesh sieve to obtain Schisandra chinensis powder, seal and store for later use;

[0056] Pulverize the camellia oleifera cake and pass through a 20-mesh sieve to obtain the camellia oleifera cake powder, which is sealed and stored for later use;

[0057] 2) Extraction: Put the southern Schisandra powder obtained in the previous step in a condensation reflux device (this device facilitates the recovery of the extractant in the subsequent vacuum distillation process), and add a mixture of ethanol and acetone with a volume ratio of 50:100 as Extractant, the ratio of solid to liquid is 1g: 50mL, after leaching at 75°C for 3.0h, cooling, filtering to take the filt...

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Abstract

The invention discloses a preparation method of a compounded fruit and vegetable cleaning agent of a kadsura longepedunculata extract and an oil-tea-cake extract. The method comprises the following steps: with an ethyl alcohol/acetone method extract of kadsura longepedunculata and an ethyl alcohol method extract of an oil-tea-cake as raw materials, combining with a resin separation technology, respectively purifying the kadsura longepedunculata extract and the oil-tea-cake extract, and purifying the extract; freeze-drying to obtain extract powder; and mixing the kadsura longepedunculata with the oil-tea-cake extract powder to obtain the compounded fruit and vegetable cleaning agent. The compounded fruit and vegetable cleaning agent is capable of cleaning unsanitary things such as soil, dirt, pesticides, germs and worm eggs on the surfaces of fruits and vegetables, does not affect the freshness of the fruits and vegetables within the shelf life, has the advantages of being high in biosecurity, low in toxicity, high in efficiency, low in amount, excellent in properties of cleaning, decontaminating and removing pesticides on the fruit and vegetable fruits, wide in bacteria and antimicrobial spectrum and high in bacteriostatic ability, is capable of cleaning dirt, microorganisms and worm eggs on the surfaces of fruits and vegetables, and does not change the nutrients and tastes of the fruits and vegetables.

Description

technical field [0001] The invention relates to a cleaning agent and a preparation method thereof, in particular to a preparation method of a fruit and vegetable cleaning agent compounded with Schisandra chinensis extract and camellia oleifera cake extract. Background technique [0002] With the rapid development of my country's agriculture, the output of fruits and vegetables has increased year by year, the scope of use of pesticides has continued to expand, and the amount of pesticides has continued to increase. Fruits and vegetables are the most consumed food in people's daily life. The amount of residual pesticides and industrial pollutants adsorbed on fruits and vegetables is large, which has already posed a serious hazard to public health. According to statistics, the pesticides ingested by humans through food accounted for more than 90% of the total amount of pesticides ingested by humans, and the pesticides ingested through eating fruits and vegetables accounted for ...

Claims

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Application Information

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IPC IPC(8): C11D7/44C11D7/60C11D10/02
Inventor 于新陈新罗维英钟蓓邱苑新江秀娟
Owner ZHONGKAI UNIV OF AGRI & ENG
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