Production of aluminium-scandium alloys
一种合金、合金化元素的技术,应用在生产铝-钪系合金领域,能够解决缓慢、追加高纯Sc金属成本等问题
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Embodiment 1
[0136] Embodiment 1: produce Al 3 Sc powder
[0137] 4Al to 1ScCl 3 The molar ratio of 5g of Al powder with an average particle size of less than 15 microns to ScCl 3 Powder mix. The material is then placed in a quartz tube and heated at a temperature between 600°C and 900°C and a pressure below 100 mbar. The temperature was first held at 600°C for 10 minutes, then increased to 650°C for 10 minutes, and to 700°C for 10 minutes, and then increased to 800°C for 10 minutes and 900°C for 10 minutes. The material is then discharged and analyzed. The product is made of Al 3 A powder composed of Sc and a small amount of Sc. Figure 8 shows the XRD spectrum of the material, clearly showing that to correspond to the Al 3 The line of Sc is dominant.
Embodiment 2
[0138] Embodiment 2: produce Al 3 Sc powder
[0139] 4Al to 1ScCl 3 The molar ratio of 5g of Al powder with an average particle size of less than 15 microns to ScCl 3 Powder mix. The material is then placed in a quartz tube and heated at a temperature between room temperature and 900° C. and a pressure below 10 mbar. The temperature was raised in steps at 100° C. and the total heating time was 60 minutes. The material is then discharged and analyzed. The product is made of Al 3 Powder composed of Sc.
Embodiment 3
[0140] Embodiment 3: produce Al 3 (Sc-Zr powder)
[0141] 4Al to 0.5ScCl 3 and 0.5ZrCl 4 The molar ratio of 5g of Al powder with an average particle size of less than 15 microns to ScCl 3 Powder and ZrCl 4Powder mix. The material is then placed in a quartz tube and heated at a temperature between room temperature and 900° C. and a pressure below 10 mbar. The temperature was raised in steps at 100° C. and the total heating time was 60 minutes. The material is then discharged and analyzed. The product is made of Al 3 (Sc-Zr) powder composition.
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