Analyzer for metal oxide film
An oxide film and analyzer technology, applied in the direction of material electrochemical variables, etc., can solve the problems of inapplicable large-scale macroscopic detection, small analysis area, and low interlayer resistance, so as to reduce the incidence of poor surface quality problems , good measurement stability and low equipment cost
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Embodiment 1
[0027] 1. Pour about 3000ml of water into the water tank 11, inject 400ml of sulfuric acid with a concentration of 8% into the acid tank 10, and immerse the acid tank in the water;
[0028] 2. The constant temperature magnetic stirrer 8 is energized, the acid is preheated, the set temperature is 40°C, and the rotation speed of the magnet 9 is 30 rpm;
[0029] 3. Connect the copper guide rod 3 to the potentiometer 1 with the wire 7, the pole plates 4 and 5 are fixed on the copper guide rod 3 by bolts, and the copper guide rod 3 is fixed on the cover plate 2 by bolts;
[0030] 4. The cover plate 2 is covered on the acid tank 10, while the pole plates 4 and 5 are immersed in the acid, and the cover plate 2 is fixed on the acid tank 10 with bolts;
[0031] 5. Turn on the potentiometer 1 to start measurement. When the value displayed on the potentiometer is stable at 0mV, the reaction is completed, and the power is turned off to end the measurement.
Embodiment 2
[0033] 1, inject about 4000ml water in the water tank 11, inject 500ml in the acid tank 10, the concentration is 10% sulfuric acid, and the acid tank 10 is immersed in water;
[0034] 2. The constant temperature magnetic stirrer 8 is energized, the acid is preheated, the set temperature is 40°C, and the rotation speed of the magnet 9 is 40 rpm;
[0035] 3. Connect the copper guide rod 3 to the potentiometer 1 with the wire 7, the pole plates 4 and 5 are fixed on the copper guide rod 3 by bolts, and the copper guide rod 3 is fixed on the cover plate 2 by bolts;
[0036] 4. The cover plate 2 is covered on the acid tank 10, while the pole plates 4 and 5 are immersed in the acid, and the cover plate 2 is fixed on the acid tank 10 with bolts;
[0037] 5. Turn on the potentiometer 1 to start measurement. When the value displayed on the potentiometer is stable at 0mV, the reaction is completed, and the power is turned off to end the measurement.
Embodiment 3
[0039] 1, inject about 4000ml water in the water tank 11, inject 600ml in the acid tank 10, the concentration is 12% sulfuric acid, and the acid tank 10 is immersed in water;
[0040] 2. The constant temperature magnetic stirrer 8 is energized, the acid is preheated, the set temperature is 40°C, and the rotation speed of the magnet 9 is 40 rpm;
[0041] 3. Connect the copper guide rod 3 to the potentiometer 1 with the wire 7, the pole plates 4 and 5 are fixed on the copper guide rod 3 by bolts, and the copper guide rod 3 is fixed on the cover plate 2 by bolts;
[0042] 4. The cover plate 2 is covered on the acid tank 10, while the pole plates 4 and 5 are immersed in the acid, and the cover plate 2 is fixed on the acid tank 10 with bolts;
[0043] 5. Turn on the potentiometer 1 to start measurement. When the value displayed on the potentiometer is stable at 0mV, the reaction is completed, and the power is turned off to end the measurement.
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