Environment-friendly high-strength high-flame-retardant polysulfide sealant, and preparation method thereof
A polysulfide sealant and high-strength technology, which is applied in the field of environment-friendly high-strength and high-flame-retardant polysulfide sealant and its preparation, can solve problems such as potential safety hazards, flammable raw materials, and reduced sealant strength
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[0057] The preparation method of described epoxymorpholine quaternary ammonium salt is: in dry three-necked bottle, first add 100ml acetocyanide, then add the N-methylmorpholine of 0.1mol and the epichlorohydrin of 0.1mol successively; After stirring, pass inert gas and heat up to 50°C, stop heating after 48 hours of reaction, filter with suction and wash the obtained epoxymorpholine quaternary ammonium salt fully with ether, then wash with acetone, fully dry in a vacuum oven for use .
[0058] Preferably, the epoxy-type quaternary ammonium salt used in the present invention is a mixture of 2,3-epoxypropyltrimethylammonium chloride and epoxymorpholine quaternary ammonium salt in a weight ratio of 1:2 to 3:1; More preferably, the epoxy-type quaternary ammonium salt used in the present invention is a mixture of 2,3-epoxypropyltrimethylammonium chloride and epoxymorpholine quaternary ammonium salt in a weight ratio of 1:1.
[0059] The applicant finds that epoxymorpholine quater...
Embodiment 1
[0110] Component A: A1100 parts, B110 parts, C120 parts, D15 parts, E11 parts, F12 parts and G11 parts. Add the above materials into a vacuum-sealed mixer or grinder, and mix thoroughly for 30 minutes.
[0111] Component B: H1100 parts, I12 parts, J110 parts, and K12 parts. Add the above materials into a vacuum-sealed mixer or grinder, and mix thoroughly for 30 minutes.
[0112] Ratio A:B=10:1, mix well. When using, mix components A (white) and B (black) uniformly in proportion, apply within 2 hours, and fully cure within 5 hours at room temperature.
Embodiment 2
[0114] Component A: A2100 parts, B110 parts, C220 parts, D25 parts, E11 parts, F22 parts and G21 parts. Add the above materials into a vacuum-sealed mixer or grinder, and mix thoroughly for 30 minutes.
[0115] Component B: H2100 parts, I12 parts, J210 parts, and K12 parts. Add the above materials into a vacuum-sealed mixer or grinder, and mix thoroughly for 30 minutes.
[0116] Ratio A:B=10:1, mix well. When using, mix components A (white) and B (black) uniformly in proportion, apply within 2 hours, and fully cure within 5 hours at room temperature.
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