Wet airflow crushing dispersion method of nanometer calcium carbonate

A technology of nano-scale calcium carbonate and airflow milling, which is applied in chemical instruments and methods, dyeing polymer organic compound treatment, inorganic pigment treatment, etc. It can solve the problems that particles are easy to agglomerate, cannot meet the application requirements, and the dispersion effect is not ideal. , to achieve the effect of fineness and remarkable effect

Inactive Publication Date: 2016-04-13
ENPING YANYI NEW MATERIALS CO LTD
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Problems solved by technology

In the calcium carbonate grinding method, there are two methods: dry method and wet method. The wet method mainly includes medium stirring and crushing technology, which has certain limitations in the fineness of particle grinding, and the dispersion effect is not ideal.
And the fineness of the wet method is much finer than that of the dry method, which can reach below 2 microns, but the smaller the particles, the easier it is to agglomerate, and such a fineness still cannot meet the needs of the application, and it cannot solve the problem of the large bulk density of the ground calcium carbonate. The problem

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  • Wet airflow crushing dispersion method of nanometer calcium carbonate

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Embodiment 1

[0021] The wet jet pulverization dispersion method of a kind of nanoscale calcium carbonate described in present embodiment 1, such as figure 1 shown, including the following steps:

[0022] (1) Dry crush the calcium carbonate ore to a powder with a fineness of 400 meshes, then mix the powder with water to make a slurry, and the proportion of the powder to the slurry is 70-75%;

[0023] (2) Add a dispersant to adjust the viscosity of the slurry;

[0024] (3) The slurry is ground by a wet medium agitating pulverizer to a particle size of less than 2 microns;

[0025] (4) Add at least one dispersant to the slurry, and enter the crushing chamber of the wet jet milling disperser. There are stators and rotors nested in each other in the crushing chamber, and the rotor drives the slurry in the crushing chamber to rotate at high speed to generate great centrifugal force and A vacuum state is formed, so that the multi-phase materials with larger particles are sucked into the working...

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Abstract

The invention discloses a wet airflow crushing dispersion method of nanometer calcium carbonate. The method comprises the following steps: carrying out dry crushing on calcium carbonate ores to form powder with the fineness of 400 meshes, mixing the powder with water to prepare a slurry, adjusting the viscosity of the slurry, grinding the adjusted slurry through a wet medium stirring crusher, introducing airflow through a wet airflow crushing dispersion machine, carrying out high-speed rotating crushing dispersion, carrying out surface active treatment, drying the obtained material, and grading the dried material to obtain a fine and stable high-quality product. Airflow dispersion is introduced in the airflow crushing dispersion method of nanometer calcium carbonate, and high pressure and high speed movement of particles forms high impact intensity and shearing stress in a specially produced crushing chamber, so liquid drops are atomized, particles are broken, the fineness of the further crushed particles reaches nanometer level, crushing and dispersion are simultaneously carried out, and the effects are substantial.

Description

technical field [0001] The invention relates to the technical field of a method for pulverizing and dispersing nano calcium carbonate, in particular to a method for wet airflow pulverizing and dispersing nano calcium carbonate. Background technique [0002] At present, ultrafine powder materials have been widely used in plastics, silicone glue, ink, insulating materials for electronic components, sealing materials and other fields. Among them, particle crushing technology and dispersion technology are very important engineering technologies. In the calcium carbonate industry, ore with high purity calcium carbonate content is widely used in various industries after repeated crushing and grinding. However, the development of grinding calcium carbonate is seriously restricted because the fineness after grinding cannot be further improved. In the calcium carbonate grinding method, there are two methods: dry method and wet method. The wet method mainly includes medium stirring a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09C1/02C09C3/04C09C3/10
CPCC09C1/021C01P2004/62C09C3/006C09C3/04C09C3/10
Inventor 潘文甄兴新谢忠吴少吟
Owner ENPING YANYI NEW MATERIALS CO LTD
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