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Method and device for monitoring service life of gas purifier

A technology of gas purification and purifier, which is applied in the direction of chemical instruments and methods, measuring devices, and testing of machine/structural components, etc. It can solve the problems of fatal safety and hidden dangers, and achieve the effect of low cost and simple monitoring process

Active Publication Date: 2017-09-19
GRIMAT ENG INST CO LTD
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

This method can effectively characterize the service life of the purifier, but it can only be applied to the life monitoring of the inert gas purifier, and there is a fatal safety hazard in the application of the hydrogen purifier, and ultra-high-purity hydrogen is an ultra-high-purity gas commonly used in the electronics industry

Method used

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  • Method and device for monitoring service life of gas purifier
  • Method and device for monitoring service life of gas purifier
  • Method and device for monitoring service life of gas purifier

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Embodiment 1

[0033] This embodiment is used to illustrate the method and device for monitoring the service life of the gas purifier in the present invention. The purifier reaction tank 2 has a diameter of 1.5mm and a length of 10cm. The loaded purification alloy filler 2-2 adopts the Ti17Zr16Mn40Cr13.5Ni13.5 purification material described in Chinese patent CN 103898389A, the particle size of the powder is -100 mesh, and the loading capacity is 50g. The structure of the monitoring device for the service life of the gas purifier and its purifier reaction tank 2 is as follows: Figure 1-2 As shown, the strain measurement uses a resistive strain gauge. The working pressure of the reaction tank 2 of the purifier is 0.5 MPa, the working temperature is 200° C., and the gas flow rate is 300 sccm. Containing 5000ppm O 2 Hydrogen was used as the raw material gas, and the gas purity was analyzed by GOW-MAC Company 592 DID gas chromatography, and the detection limit of impurity gas was 10ppb. The ...

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Abstract

The invention relates to a method of monitoring a service lifetime of a gas purifier and a device thereof. According to the method, gas is fed into a purifier reacting tank after the gas flow rate F is measured through a flowmeter, purified gas flows out through a gas outlet, tank strain Epsilon is measured through a strain gage, temperature T of the outer surface or the inside of the purifier reacting tank is measured by a temperature sensor, pressure P of the outlet is measured by a pressure sensor, the gas flow rate F, the tank strain Epsilon, the temperature T and the pressure P are sent to a control unit, the measured tank strain Epsilon is rectified according to the real-time temperature T and the real-time pressure P to obtain real strain [Epsilon]R, and the control unit monitors the service lifetime according to the gas flow rate F and the real strain [Epsilon]R and outputs indicator signals to a service lifetime indicator. Real-time service lifetime monitoring for a purifier can be achieved in a low cost through the method and the device, and is free of influences of working conditions such as using pressure and a flow rate, or is influenced by the working conditions such as the using pressure and the flow rate in a controllable manner. The method and the device can be widely used for service lifetime monitoring for gas purifiers for He, Ne, Ar, Kr, Xe, N2, H2, and the like.

Description

technical field [0001] The invention belongs to the technical field of service life monitoring of a gas purifier, and in particular relates to a method and a device for monitoring the service life of a gas purifier. Background technique [0002] High-purity gases are widely used in the electronics industry, such as large-scale integrated circuits, liquid crystal displays, solar cells, LEDs, optical fibers and other production processes, which require a large amount of high-purity gases. In some applications, there are extremely strict requirements on the purity of the gas. For example, in the MOCVD epitaxial growth process of LEDs, a large amount of H 2 and N 2 , and it is usually required that the purity of the gas before entering the equipment is above 8N (99.999999%), that is, the impurity content in the gas is less than 10ppb (1ppb=10 -9 ). In order to meet the above gas purity requirements, it is usually necessary to use a gas purifier. [0003] Common gas purifiers...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D46/00B01D53/04B01D46/42G01M13/00
CPCB01D46/00B01D46/42B01D53/04G01M13/00
Inventor 邱昊辰郭秀梅李志念叶建华袁宝龙王树茂刘晓鹏蒋利军
Owner GRIMAT ENG INST CO LTD
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