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Heavy oil emulsifying viscosity reducer synthesis process based on sulfonation degree control

A technology of emulsification viscosity reduction and synthesis process, applied in the direction of drilling compositions, chemical instruments and methods, etc., can solve the problems of complex production process, unsuitable for large-scale production, low production efficiency, etc. Effects of improving single-pass conversion rate and product yield, and improving work efficiency

Inactive Publication Date: 2016-06-08
吕艳
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Problems solved by technology

In the current synthesis process method of emulsified viscosity reducer, the technological process is not easy to implement, the finished product of viscous oil emulsified viscosity reducer has low purity, the single-pass conversion rate of reactants is low, the production process is complicated, the production efficiency is low, and the cost is high. suitable for mass production

Method used

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Embodiment

[0011] The heavy oil emulsified viscosity reducer synthesis process based on controlling the degree of sulfonation of the present embodiment comprises the following steps:

[0012] (1) Condensation reaction of octylphenol polyoxyethylene ether and formaldehyde;

[0013] (2) The sulfonation reaction of the co-condensation polymer and concentrated sulfuric acid, and the degree of sulfonation during the reaction process is controlled to be 0.95;

[0014] (3) Final neutralization to obtain viscous oil emulsified viscosity reducer.

[0015] Based on the synthesis process of thick oil emulsified viscosity reducer based on the control of sulfonation degree, there is no need for tedious post-reaction treatment, the process is simple and feasible, and it is environmentally friendly and pollution-free. The process is easy to implement, the production cost is low, and the synthesis yield is high. Industrial production.

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Abstract

The present invention discloses a heavy oil emulsifying viscosity reducer synthesis process based on sulfonation degree control. The heavy oil emulsifying viscosity reducer synthesis process comprises: (1) carrying out a condensation reaction of octyl phenol polyoxyethylene ether and formaldehyde; (b) carrying out a sulfonation reaction of a co-polycondensate and concentrated sulfuric acid, and controlling the sulfonation degree during the reaction process at 0.70-0.95; and (c) neutralizing to prepare the heavy oil emulsifying viscosity reducer. According to the present invention, the heavy oil emulsifying viscosity reducer is successfully synthesized, the synthesis efficiency is high, the synthesis cost is low, and by controlling the sulfonation degree during the reaction process, the product stability is improved.

Description

technical field [0001] The invention belongs to the technical field of chemical synthesis, and in particular relates to a synthesis process of a thick oil emulsification viscosity reducer based on controlling the degree of sulfonation. Background technique [0002] There are many types of viscosity reducers. Among them, the effect of polyether viscosity reducer is better. ME dryness reducer can play the following roles: (1) Reduce the paste viscosity, adding 1 part of ME viscosity reducer per 100 parts of PVC paste resin can reduce the paste viscosity by 1 / 3~1 / 2. For high-speed coating, slush molding, dipping, dipping and other molding processes that require low-viscosity PVC paste, adding a viscosity reducer is an effective method for reducing viscosity. (2) The effect of reducing the amount of plasticizer on reducing the viscosity of the paste, the effect of 1 part of ME viscosity reducer is equivalent to 6-8 parts of DOP. Therefore, for products that require higher h...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08G65/331C08G65/326C09K8/584C09K8/588
Inventor 吕艳
Owner 吕艳
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