Hypodermic injection in-situ gel for treating osteosarcomas
A technology of subcutaneous injection and in situ gel, applied in the field of medicine, can solve the problems of less than 20% survival rate and inconvenient life of patients
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Embodiment 1
[0023] Example 1 Preparation of in situ gel for subcutaneous injection for the treatment of osteosarcoma
[0024] 1) Take 280g of doxorubicin hydrochloride and 20g of HIV-1-TAT protein 47-57 polypeptide fragment, add deionized water to make preparation A, and the concentration of doxorubicin in preparation A is 10mg / ml;
[0025] 2) Add poloxamer P407, poloxamer P188, and hydroxypropyl methylcellulose K4M to the solution A in sequence, stir well, and disperse evenly to obtain the solution B. The amount of poloxamer P407 in the solution B is The percentage by weight is 20%, the percentage by weight of Poloxamer P188 is 1.2%, and the percentage by weight of hydroxypropyl methylcellulose K4M is 0.3%;
[0026] 3) Swell the solution B at 4°C for 24 hours, pass it through a 0.22 μm microporous membrane, and dispense it.
Embodiment 2
[0027] Example 2 Preparation of in situ gel for subcutaneous injection for the treatment of osteosarcoma
[0028] 1) Take 480g of doxorubicin hydrochloride and 30g of HIV-1-TAT protein 47-57 polypeptide fragment, add deionized water to make a solution A, and the concentration of doxorubicin in the solution A is 10mg / ml;
[0029] 2) Add poloxamer P407, poloxamer P188, and hydroxypropyl methylcellulose K4M to the solution A in sequence, stir well, and disperse evenly to obtain the solution B. The amount of poloxamer P407 in the solution B is The percentage by weight is 20%, the percentage by weight of Poloxamer P188 is 1.2%, and the percentage by weight of hydroxypropyl methylcellulose K4M is 0.3%;
[0030] 3) Swell the solution B at 4°C for 24 hours, pass it through a 0.22 μm microporous membrane, and dispense it.
Embodiment 3
[0031] Example 3 Preparation of in situ gel for subcutaneous injection for the treatment of osteosarcoma
[0032] 1) Take 340g of doxorubicin hydrochloride and 20g of HIV-1-TAT protein 47-57 polypeptide fragments, add deionized water to make solution A, and the concentration of doxorubicin in solution A is 10mg / ml;
[0033] 2) Add poloxamer P407, poloxamer P188, and hydroxypropyl methylcellulose K4M to the solution A in sequence, stir well, and disperse evenly to obtain the solution B. The amount of poloxamer P407 in the solution B is The percentage by weight is 20%, the percentage by weight of Poloxamer P188 is 1.2%, and the percentage by weight of hydroxypropyl methylcellulose K4M is 0.3%;
[0034] 3) Swell the solution B at 4°C for 24 hours, pass it through a 0.22 μm microporous membrane, and dispense it.
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