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Normal-temperature synthesis method of electronic-grade high-purity barium carbonate

A high-purity barium carbonate synthesis technology at room temperature, which is applied in the direction of barium carbonate, calcium carbonate/strontium/barium, etc., can solve the problems of high production energy consumption, large emissions, and high costs, and achieve energy saving, water conservation, and emission reduction Effect

Active Publication Date: 2016-06-29
BAOJI QINLONG ELECTRONICS SCI & TECH CO LTD
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AI Technical Summary

Problems solved by technology

[0002] Electronic grade high-purity barium carbonate is a material that requires high content, low impurities, and small and uniform particle size. Generally, production is carried out at above 60°C, which results in high energy consumption, large emissions, and high costs.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0029] The first step, barium chloride is dissolved and purified. Add 600kg of pure water into the barium dissolving tank, start stirring at normal temperature, slowly add 150kg of barium chloride dihydrate to fully dissolve, adjust the pH value of the solution with solid barium hydroxide to not less than 10, and then stir for 1 hour, The solution is pumped into a precipitation tank for precipitation for 24 hours, and the barium chloride solution obtained after filtering the supernatant is put into a reserve tank for subsequent use. The sediment is accumulated to a certain amount before being processed.

[0030] The second step, the synthesis of barium carbonate. Add 775kg of pure water into the ammonium dissolving tank, start stirring at room temperature, slowly add 117kg of food-grade ammonium bicarbonate, make it fully dissolved and then filter, pump the filtrate into the synthesis tank, under the premise of strong stirring, press 7.5kg Add the standby barium chloride sol...

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PUM

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Abstract

The invention discloses a normal-temperature synthesis method of electronic-grade high-purity barium carbonate.The method comprises the steps of barium carbonate dissolution and purification, barium carbonate synthesis and barium carbonate washing and purification.A purified barium carbonate solution is dropwise added into a food-grade ammonium bicarbonate solution under the normal temperature to synthesize barium carbonate, and the washing frequency of the barium carbonate is reduced to three.The synthesis temperature of the high-purity barium carbonate is reduced from the traditional 60 DEG C to normal temperature; on the basis of ensuring that the synthesized barium carbonate meets the electronic-grade high-purity requirement, energy is saved, emission is reduced, and the cost is reduced.

Description

technical field [0001] The invention belongs to the technical field of electronic materials, and in particular relates to a method for synthesizing electronic-grade high-purity barium carbonate at room temperature. Background technique [0002] Electronic grade high-purity barium carbonate is a material that requires high content, low impurities, and small and uniform particle size. Generally, production is carried out at above 60°C, which results in high energy consumption, large emissions, and high costs. . As the requirements for the environment are getting higher and higher, and in order to achieve energy saving and emission reduction and reduce production costs, if barium carbonate can be synthesized under normal temperature conditions, it can also achieve electronic grade high purity (that is, high content, low impurities, and small particle size) And uniform) requirements are very necessary. Contents of the invention [0003] The technical problem solved by the pr...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01F11/18
CPCC01F11/188C01P2006/80
Inventor 董选明
Owner BAOJI QINLONG ELECTRONICS SCI & TECH CO LTD
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